Near-ambient pressure x-ray photoelectron spectroscopy (NAP-XPS) is a less traditional form of XPS that allows samples to be analyzed at relatively high pressures, i.e., greater than 2500 Pa. With NAP-XPS, XPS can analyze moderately volatile liquids, biological samples, porous materials, and/or polymeric materials that outgas significantly. In this submission, we show C 1s, O 1s, and survey NAP-XPS spectra from ethylene glycol, an organic solvent that could not be analyzed at near-ambient pressures by conventional approaches. An N 1s signal is present in the survey spectrum of the material.
REFERENCES
1.
S. A.
Voelkel
and Y. X.
Hu
, Theriogenology
37
, 687
(1992
). 2.
R.
Saint-Loup
, T.
Jeanmaire
, J.-J.
Robin
, and B.
Boutevin
, Polymer
44
, 3437
(2003
). 3.
R.
Saint-Loup
, J.-J.
Robin
, B.
Boutevin
, M.
Argalon
, and A.
Michel
, Macromol. Chem. Phys.
203
, 1249
(2002
). 4.
A.
Broderick
, Y.
Khalifa
, M. B.
Shiflett
, and J. T.
Newberg
, J. Phys. Chem. C
121
, 7337
(2017
). 5.
M. T.
Camci
, B.
Ulgut
, C.
Kocabas
, and S.
Suzer
, J. Phys. Chem. C
122
, 11883
(2018
). 6.
E. F.
Smith
, F. J. M.
Rutten
, I. J.
Villar-Garcia
, D.
Briggs
, and P.
Licence
, Langmuir
22
, 9386
(2006
). 7.
T. G.
Avval
, S.
Bahr
, M.
Meyer
, P.
Dietrich
, A.
Thißen
, and M. R.
Linford
, Surf. Sci. Spectra
26
, 014020
(2019
). 8.
D.
Shah
, D. I.
Patel
, S.
Bahr
, M.
Meyer
, P.
Dietrich
, A.
Thißen
, and M. R.
Linford
, Surf. Sci. Spectra
26
, 024003
(2019
).9.
D.
Shah
, C. V.
Cushman
, S.
Bahr
, P.
Dietrich
, M.
Meyer
, A.
Thißen
, and M. R.
Linford
, Surf. Sci. Spectra
26
, 024005
(2019
).10.
V.
Jain
, S.
Bahr
, M.
Meyer
, P.
Dietrich
, A.
Thißen
, and M. R.
Linford
, Surf. Sci. Spectra
26
, 014027
(2019
). 11.
T.
Roychowdhury
, C. V.
Cushman
, R. A.
Synowicki
, and M. R.
Linford
, Surf. Sci. Spectra
25
, 026001
(2018
). 12.
H.
Siegbahn
, J. Phys. Chem.
89
, 897
(1985
). 13.
D. I.
Patel
et al., Surf. Sci. Spectra
26
, 016801
(2019
). 14.
C.
Rodriguez
, P.
Dietrich
, V.
Torres-Costa
, V.
Cebrián
, C.
Gómez-Abad
, A.
Díaz
, O.
Ahumada
, and M. M.
Silván
, Appl. Surf. Sci.
492
, 36 (2019
).15.
M.
Kjærvik
, K.
Schwibbert
, P.
Dietrich
, A.
Thissen
, and W. E. S.
Unger
, Surf. Interface Anal.
50
, 996
(2018
). 16.
M.
Kjærvik
, A.
Hermanns
, P.
Dietrich
, A.
Thissen
, S.
Bahr
, B.
Ritter
, E.
Kemnitz
, and W. E. S.
Unger
, J. Phys.: Condens. Matter
29
, 474002
(2017
). 17.
P. M.
Dietrich
, S.
Bahr
, T.
Yamamoto
, M.
Meyer
, and A.
Thissen
, J. Electron Spectrosc. Relat. Phenom.
231
, 118
(2019
). 18.
V.
Jain
, M. C.
Biesinger
, and M. R.
Linford
, Appl. Surf. Sci.
447
, 548
(2018
). 19.
M. P.
Seah
, Surf. Sci.
420
, 285
(1999
). 20.
H.
Siegbahn
, L.
Asplund
, P.
Kelfve
, and K.
Siegbahn
, J. Electron. Spectrosc. Relat. Phenom.
7
, 411
(1975
). 21.
S.
Tougaard
, Surf. Interface Anal.
50
, 657
(2018
). 22.
D.
Shah
, D. I.
Patel
, T.
Roychowdhury
, G. B.
Rayner
, N.
O’Toole
, D. R.
Baer
, and M. R.
Linford
, J. Vac. Sci. Technol. B
36
, 062902
(2018
). © 2019 Author(s).
2019
Author(s)
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