Near-ambient pressure x-ray photoelectron spectroscopy (NAP-XPS) is a less traditional form of XPS that allows samples to be analyzed at relatively high pressures, i.e., greater than 2500 Pa. With NAP-XPS, XPS can probe moderately volatile liquids, biological samples, porous materials, and/or polymeric materials that outgas significantly. In this submission, we show the survey, O 1s, valence band, and O KLL Auger NAP-XPS spectra of oxygen gas, O2, a material that would be difficult to analyze by conventional XPS. A small N 1s signal from N2(g) is also observed in the survey spectrum. The O 1s narrow scan is fit to Gaussian-Lorentzian sum functions. The Lorentzian character of this synthetic line shape was varied to obtain the best fit. Since it is likely that O2(g) will be present in other NAP-XPS analyses, these data should serve as a useful reference for other researchers.
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June 2019
Research Article|
July 11 2019
Oxygen gas, O2(g), by near-ambient pressure XPS
Tahereh G. Avval;
Tahereh G. Avval
1
Department of Chemistry and Biochemistry, Brigham Young University
, C100 BNSN, Provo, Utah 84602
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Shiladitya Chatterjee;
Shiladitya Chatterjee
1
Department of Chemistry and Biochemistry, Brigham Young University
, C100 BNSN, Provo, Utah 84602
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Grant T. Hodges;
Grant T. Hodges
1
Department of Chemistry and Biochemistry, Brigham Young University
, C100 BNSN, Provo, Utah 84602
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Stephan Bahr;
Stephan Bahr
2
SPECS Surface Nano Analysis GmbH
, Voltastrasse 5, 13355 Berlin, Germany
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Paul Dietrich
;
Paul Dietrich
2
SPECS Surface Nano Analysis GmbH
, Voltastrasse 5, 13355 Berlin, Germany
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Michael Meyer;
Michael Meyer
2
SPECS Surface Nano Analysis GmbH
, Voltastrasse 5, 13355 Berlin, Germany
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Andreas Thißen;
Andreas Thißen
2
SPECS Surface Nano Analysis GmbH
, Voltastrasse 5, 13355 Berlin, Germany
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Matthew R. Linford
Matthew R. Linford
a)
1
Department of Chemistry and Biochemistry, Brigham Young University
, C100 BNSN, Provo, Utah 84602
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a)
Electronic mail: mrlinford@chem.byu.edu
Surf. Sci. Spectra 26, 014021 (2019)
Article history
Received:
April 22 2019
Accepted:
June 14 2019
Citation
Tahereh G. Avval, Shiladitya Chatterjee, Grant T. Hodges, Stephan Bahr, Paul Dietrich, Michael Meyer, Andreas Thißen, Matthew R. Linford; Oxygen gas, O2(g), by near-ambient pressure XPS. Surf. Sci. Spectra 1 June 2019; 26 (1): 014021. https://doi.org/10.1116/1.5100962
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