Strain-balanced InAs/InAs1−xSbx type-II superlattices (SLs) have been proposed for possible long-wavelength infrared applications. This paper reports a detailed structural characterization study of InAs/InAs1−xSbx SLs with varied Sb composition grown on GaSb (001) substrates by modulated and conventional molecular beam epitaxy (MBE). X-ray diffraction was used to determine the SL periods and the average composition of the InAs1−xSbx alloy layers. Cross-section transmission electron micrographs revealed the separate In(As)Sb/InAs(Sb) ordered-alloy layers within individual InAs1−xSbx layers for SLs grown by modulated MBE. For the SLs grown by conventional MBE, examination by high-resolution electron microscopy revealed that interfaces for InAs1−xSbx deposited on InAs were more abrupt, relative to InAs deposited on InAs1−xSbx: this feature was attributed to Sb surfactant segregation occurring during the SL growth. Overall, these results establish that strain-balanced SL structures with excellent crystallinity can be achieved with proper design (well thickness versus Sb composition) and suitably optimized growth conditions.

1.
G. A.
Sai-Halasz
,
R.
Tsu
, and
L.
Esaki
,
Appl. Phys. Lett.
30
,
651
(
1977
).
2.
D. L.
Smith
,
T. C.
McGill
, and
J. N.
Schulman
,
Appl. Phys. Lett.
43
,
180
(
1983
).
3.
D. L.
Smith
and
C.
Mailhiot
,
J. Appl. Phys.
62
,
2545
(
1987
).
4.
D. N.
Talwar
and
J. P.
Loehr
,
Phys. Rev. B
49
,
10345
(
1994
).
5.
C. H.
Grein
,
P. M.
Young
, and
H.
Ehrenreich
,
Appl. Phys. Lett.
61
,
2905
(
1992
).
6.
D. H.
Chow
,
R. H.
Miles
,
T. C.
Hasenberg
,
A. R.
Kost
,
Y.-H.
Zhang
,
H. L.
Dunlap
, and
L.
West
,
Appl. Phys. Lett.
67
,
3700
(
1995
).
7.
J. L.
Johnson
,
L. A.
Samoska
,
A. C.
Gossard
,
J. L.
Merz
,
M. D.
Jack
,
G. R.
Chapman
,
B. A.
Baumgratz
,
K.
Kosai
, and
S. M.
Johnson
,
J. Appl. Phys.
80
,
1116
(
1996
).
8.
H.
Mohseni
,
M.
Razeghi
,
G. J.
Brown
, and
Y. S.
Park
,
Appl. Phys. Lett.
78
,
2107
(
2001
).
9.
A.
Hood
,
D.
Hoffman
,
B.-M.
Nguyen
,
P.-Y.
Delaunay
,
E.
Michel
, and
M.
Razeghi
,
Appl. Phys. Lett.
89
,
093506
(
2006
).
10.
G. C.
Osbourn
,
J. Vac. Sci. Technol. B
2
,
176
(
1984
).
11.
Y.-H.
Zhang
,
Appl. Phys. Lett.
66
,
118
(
1995
).
12.
D.
Lackner
,
O. J.
Pitts
,
M.
Steger
,
A.
Yang
,
M. L. W.
Thewalt
, and
S. P.
Watkins
,
Appl. Phys. Lett.
95
,
081906
(
2009
).
13.
Y.
Huang
,
J.-H.
Ryou
,
R. D.
Dupuis
,
V. R.
D’Costa
,
E. H.
Steenbergen
,
J.
Fan
,
Y.-H.
Zhang
,
A.
Petschke
,
M.
Mandl
, and
S.-L.
Chuang
,
J. Cryst. Growth
314
,
92
(
2011
).
14.
E. H.
Steenbergen
,
Y.
Huang
,
J.-H.
Ryou
,
L.
Ouyang
,
J.-J.
Li
,
D. J.
Smith
,
R. D.
Dupuis
, and
Y.-H.
Zhang
,
Appl. Phys. Lett.
99
,
071111
(
2011
).
15.
W.
Walukiewicz
,
Mater. Res. Soc. Symp. Proc.
148
,
137
(
1989
).
16.
C. H.
Grein
,
M. E.
Flatte
, and
H.
Ehrenreich
,
Proceedings on the Third International Symposium on Long Wavelength Infrared Detectors and Arrays: Physics and Applications III
,
Chicago, IL
, 8–13 October 1995 (Electrochemical Society, Pennington,
1995
), p.
211
.
17.
E. H.
Steenbergen
,
B. C.
Connelly
,
G. D.
Metcalfe
,
H.
Shen
,
M.
Wraback
,
D.
Lubyshev
,
Y.
Qiu
,
J. M.
Fastenau
,
A. W. K.
Liu
,
S.
Elhamri
,
O. O.
Cellek
, and
Y.-H.
Zhang
, Appl. Phys. Lett. (in press).
18.
Y.-H.
Zhang
,
J. Cryst. Growth
150
,
838
(
1995
).
19.
Y.-H.
Zhang
and
D. H.
Chow
,
Appl. Phys. Lett.
65
,
3239
(
1994
).
20.
A. Y.
Lew
,
E. T.
Yu
, and
Y.-H.
Zhang
,
J. Vac. Sci. Technol. B
14
,
2940
(
1996
).
21.
Y.-H.
Zhang
,
A.
Lew
,
E.
Yu
, and
Y.
Chen
,
J. Cryst. Growth
175
,
833
(
1997
).
22.
E.
Hall
,
H.
Kroemer
, and
L. A.
Coldren
,
J. Cryst. Growth
203
,
447
(
1999
).
23.
R.
Kaspi
and
G. P.
Donati
,
J. Cryst. Growth
251
,
515
(
2003
).
24.
K.
Muraki
,
S.
Fukatsu
,
Y.
Shiraki
, and
R.
Ito
,
Appl. Phys. Lett.
61
,
557
(
1992
).
25.
P. M.
Young
and
H.
Ehrenreich
,
Appl. Phys. Lett.
61
,
1069
(
1992
).
26.
E. H.
Steenbergen
,
K.
Nunna
,
L.
Ouyang
,
B.
Ullrich
,
D. L.
Huffaker
,
D. J.
Smith
, and
Y.-H.
Zhang
,
J. Vac. Sci. Technol. B
(to be published
27.
C. Z.
Wang
,
D. J.
Smith
,
S.
Tobin
,
T.
Parodos
,
J.
Zhao
,
Y.
Chang
, and
S.
Sivananthan
,
J. Vac. Sci. Technol. A
24
,
995
(
2006
).
28.
J.
Steinshnider
,
J.
Harper
,
M.
Weimer
,
C.-H.
Lin
,
S. S.
Pei
, and
D. H.
Chow
,
Phys. Rev. Lett.
85
,
4562
(
2000
).
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