Both selective and nonselective focused ion beam (FIB) processes have become critical for enabling fine-scale activities such as nano-machining and nano-fabrication in compound material removal applications. In this paper, we investigate the influence of FIB ion acceleration voltage on gas assisted etch rates for the most frequently used materials in the microelectronic industry, using common FIB etchants. These results can serve as a baseline for FIB process development using various materials for both highly-selective and (almost) nonselective material removal. Etching strategies are suggested. Two test cases are presented here, in which we performed either selective or nonselective material removal processes. The etch rate of different materials was found to be dependent on acceleration voltage, and very specific to the material-precursor system.

1.
N.
Yao
,
Focused ion Beam Systems- Basics and Applications
(
Cambridge University
,
Cambridge, England
,
2007
), p.
268
.
2.
J.
Orloff
,
M.
Utlaut
, and
L.
Swanson
,
High Resolution Focused Ion Beam
(
Kluwer Academic
,
New York
,
2003
), p.
136
.
3.
A. A.
Tseng
,
Small
1
,
924
(
2005
).
4.
S.
Reyntjens
and
R.
Puers
,
J. Micromech. Microeng.
11
,
287
(
2001
).
5.
S.
Haehn
and
T. S.
Kalkur
,
J. Electron. Test.
11
,
273
(
1997
).
6.
D. M.
Donnet
and
H.
Roberts
,
Microscopy of Semiconducting Materials
(
Springer-Verlag
,
Berlin
,
2005
), pp.
403
408
.
7.
R.
Young
and
M. V.
Moore
,
Introduction to Focused Ion Beams
(
Springer
,
New York
,
2005
), pp.
247
268
.
8.
L.
Giannuzzi
,
J. L.
Brown
,
S. R.
Brown
,
R. B.
Irvin
, and
F. A.
Stevie
,
Microsc. Res. Tech.
41
,
285
(
1998
).
9.
L.
Giannuzzi
,
B. W.
Kempshall
,
S. M.
Schwartz
,
J. K.
Lomness
,
B. I.
Prenitzer
, and
F. A.
Stevie
,
Introduction to Focused Ion Beams
(
Springer
,
New York
,
2005
), pp.
201
228
.
10.
T.
Kamino
,
T.
Yaguchi
,
T.
Hashimoto
,
T.
Ohnishi
, and
K.
Umemura
,
Introduction to Focused Ion Beams
(
Springer
,
New York
,
2005
), pp.
229
245
.
11.
J.
Melngailis
,
J. Vac. Sci. Technol. B
5
,
469
(
1987
).
12.
K. N.
Hooghan
,
Introduction to Focused Ion Beams Insturmentation, Theory, Techniques and Practice
, edited by
L. A.
Giannuzzi
and
F. A.
Stevie
(
Springer
,
New York
,
2005
), pp.
87
106
.
13.
Y.
Fu
,
Ion Beam in Nanoscience and Technology
, edited by
R.
Hellborg
,
H. J.
Whitlow
, and
Y.
Zhang
(
Springer
,
Berlin
,
2009
), pp.
293
296
.
14.
D.
Josephson
and
B.
Gottlieb
,
Advances in Electronic Testing: Challenges and Methodologies
(
Springer
,
New York
,
2006
), pp.
77
108
.
15.
C.
Rue
,
S.
Herschbein
, and
C.
Scrudato
,
Proc. ISTFA
34
,
141
(
2008
).
16.
S. K.
Islam
and
M. R.
Haider
,
Sensors and Low Power Signal Processing
(
Springer
,
New York
,
2010
), pp.
19
30
.
17.
J.
Chen
,
D.
Yang
, and
D.
Que
,
Front. Mater. Sci. China
,
2
,
335
(
2008
).
18.
R. L.
Rhoades
,
Future Fab Int.
24
,
77
(
2008
).
19.
T.
Osaka
and
M.
Yoshino
,
Electrochemical Nanotechnologies
(
Springer
,
New York
,
2010
), pp.
255
274
.
20.
B.
Li
,
T. D.
Sullivan
,
T. C.
Lee
, and
D.
Badami
,
Microelectron. Reliab.
44
,
365
(
2004
).
21.
P. J.
Ireland
,
Thin Solid Films
304
,
1
(
1997
).
22.
A.
Grill
and
V.
Patel
,
Appl. Phys. Lett.
79
,
803
(
2001
).
23.
E.
Andideh
,
M.
Lerner
,
G.
Palmrose
,
S.
El-Mansy
,
T.
Scherban
,
G.
Xu
, and
J.
Blaine
,
J. Vac. Sci. Technol. B
22
,
196
(
2004
).
24.
R. H.
Livengood
,
P.
Winer
, and
V. R.
Rao
,
J. Vac. Sci. Technol. B
17
,
40
(
1999
).
25.
M.
Paniccia
,
T.
Eiles
,
R.
Livengood
,
V. R. M.
Rao
,
P.
Winer
,
W. M.
Yee
,
Microelectron. Eng.
46
,
27
(
1999
).
26.
J. D.
Casey
,
M.
Phaneuf
,
C.
Chandler
,
M.
Megorden
,
K. E.
Noll
,
R.
Schuman
,
T. J.
Gannon
,
A.
Krechmer
,
D.
Monforte
,
N.
Antoniou
,
N.
Bassom
,
J.
Li
,
P.
Carleson
, and
C.
Huynh
,
J. Vac. Sci. Technol. B
20
,
2682
(
2002
).
27.
C.
Rue
,
R.
Shapherd
,
R.
Hallstein
, and
R.
Livengood
,
Proc. ISTFA
33
,
312
(
2007
).
28.
K.
Sugano
and
O.
Tabata
,
J. Micromech. Microeng.
12
,
911
(
2002
).
29.
H. F.
Winters
,
J. Vac. Sci. Technol. B
1
,
927
(
1983
).
30.
S. B.
Herschbein
,
L. S.
Fischer
,
T. L.
Kane
,
M. P.
Tenney
, and
A. D.
Shore
,
Proc. ISTFA
24
,
127
(
1998
).
31.
R. A.
Lee
,
P.
Wolpert
, and
A.
Pednekar
,
Proc. ISTFA
27
,
285
(
2001
).
32.
K.
Gamo
and
S.
Namba
,
J. Vac. Sci. Technol. B
8
,
1927
(
1990
).
33.
L.
Frey
,
C.
Lehrer
, and
H.
Ryssel
,
Appl. Phys. A
76
,
1017
(
2003
).
34.
T.
Lundquist
and
M.
Thompson
,
Microelectronics Failure Analysis, Desk Reference 5th Edition
(
ASM International
,
Materials Park, OH
,
2004
), p.
58
.
35.
F.
Mosselveld
,
V. V.
Makarov
,
T. R.
Lundquist
,
D. P.
Griffis
, and
P. E.
Russel
,
J. Microsc.
214
,
246
(
2004
).
36.
J. P.
Biersack
and
L. G.
Haggmark
,
Nucl. Instrum. Methods Phys. Res. B
174
,
257
(
1980
).
37.
J. R.
Phillips
,
D. P.
Griffis
, and
P. E.
Russell
,
J. Vac. Sci. Technol. A
18
,
1061
(
2000
).
38.
L. R.
Harriott
,
Jpn. J. Appl. Phys.
33
,
7094
(
1994
).
39.
H. B.
Kim
,
G.
Hobler
,
A.
Lugstein
, and
E.
Bertagnolli
,
J. Micromech. Microeng.
17
,
1178
(
2007
).
40.
T. L.
Matteson
,
S. W.
Schwartz
,
E. C.
Houge
,
B. W.
Kempshall
, and
L. A.
Giannuzzi
,
J. Electron. Mater.
31
,
33
(
2002
).
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