We investigate intermittent plasticity in nanopillars of nanocrystalline molybdenum based on in situ transmission electron microscopy observations. By correlating electron imaging results with the measured nanopillar mechanical response, we demonstrate that the intermittent plasticity in nanocrystalline molybdenum is largely caused by dislocation avalanches. Electron imaging further reveals three types of dislocation avalanches, from intragranular to transgranular to cross-granular avalanches. The measured strain bursts resulted from avalanches have similar magnitudes to those reported for the molybdenum single-crystal pillars, while the corresponding flow stress in nanocrystalline molybdenum is greatly enhanced by the small grain size. Statistical analysis also shows that the avalanches behavior has similar characteristic as single crystals in the mean field theory model. Together, our findings here provide critical insights into the deformation mechanisms in a nanostructured body-centered-cubic metal.

1.
F. F.
Csikor
,
C.
Motz
,
D.
Weygand
,
M.
Zaiser
, and
S.
Zapperi
,
Science
318
,
251
(
2007
).
2.
R.
Maaß
and
P. M.
Derlet
,
Acta Mater.
143
,
338
(
2018
).
3.
M. D.
Uchic
,
P. A.
Shade
, and
D. M.
Dimiduk
,
Annu. Rev. Mater. Res.
39
,
361
(
2009
).
4.
D. M.
Dimiduk
,
C.
Woodward
,
R.
LeSar
, and
M. D.
Uchic
,
Science
312
,
1188
(
2006
).
5.
J. R.
Greer
and
J. T. M.
De Hosson
,
Prog. Mater. Sci.
56
,
654
(
2011
).
6.
M.
Zaiser
,
J.
Schwerdtfeger
,
A. S.
Schneider
,
C. P.
Frick
,
B. G.
Clark
,
P. A.
Gruber
, and
E.
Arzt
,
Philos. Mag.
88
,
3861
(
2008
).
7.
S.
Brinckmann
,
J.-Y.
Kim
, and
J. R.
Greer
,
Phys. Rev. Lett.
100
,
155502
(
2008
).
8.
N.
Friedman
,
A. T.
Jennings
,
G.
Tsekenis
,
J.-Y.
Kim
,
M.
Tao
,
J. T.
Uhl
,
J. R.
Greer
, and
K. A.
Dahmen
,
Phys. Rev. Lett.
109
,
095507
(
2012
).
10.
M. D.
Uchic
,
D. M.
Dimiduk
,
J. N.
Florando
, and
W. D.
Nix
,
Science
305
,
986
(
2004
).
11.
X. W.
Gu
,
C. N.
Loynachan
,
Z.
Wu
,
Y.-W.
Zhang
,
D. J.
Srolovitz
, and
J. R.
Greer
,
Nano Lett.
12
,
6385
(
2012
).
12.
Y.
Zou
,
J. M.
Wheeler
,
H.
Ma
,
P.
Okle
, and
R.
Spolenak
,
Nano Lett.
17
,
1569
(
2017
).
13.
T.
Richeton
,
J.
Weiss
, and
F.
Louchet
,
Nat. Mater.
4
,
465
(
2005
).
14.
T.
Niiyama
and
T.
Shimokawa
,
Phys. Rev. B
94
,
140102
(
2016
).
15.
H.-W.
Hsiao
,
S.
Li
,
K. A.
Dahmen
, and
J.-M.
Zuo
,
Phys. Rev. Mater.
3
,
083601
(
2019
).
16.
P.
Zhang
,
J.-J.
Bian
,
J.-Y.
Zhang
,
G.
Liu
,
J.
Weiss
, and
J.
Sun
,
Mater. Des.
188
,
108444
(
2020
).
17.
C. S.
Kaira
,
S. S.
Singh
,
A.
Kirubanandham
, and
N.
Chawla
,
Acta Mater.
120
,
56
(
2016
).
18.
J. R.
Greer
,
D.
Jang
, and
X. W.
Gu
,
JOM
64
,
1241
(
2012
).
19.
K. Y.
Xie
,
S.
Shrestha
,
Y.
Cao
,
P. J.
Felfer
,
Y.
Wang
,
X.
Liao
,
J. M.
Cairney
, and
S. P.
Ringer
,
Acta Mater.
61
,
439
(
2013
).
20.
Y.
Hu
,
L.
Shu
,
Q.
Yang
,
W.
Guo
,
P. K.
Liaw
,
K. A.
Dahmen
, and
J.-M.
Zuo
,
Commun. Phys.
1
,
61
(
2018
).
21.
J.-M.
Zuo
, in
Springer Handbook of Microscopy
, edited by
P. W.
Hawkes
and
J. C. H.
Spence
(
Springer International Publishing
,
Cham
,
2019
), p.
905
.
22.
A. S.
Schneider
,
D.
Kaufmann
,
B. G.
Clark
,
C. P.
Frick
,
P. A.
Gruber
,
R.
Mönig
,
O.
Kraft
, and
E.
Arzt
,
Phys. Rev. Lett.
103
,
105501
(
2009
).
23.
J.-Y.
Kim
,
D.
Jang
, and
J. R.
Greer
,
Acta Mater.
58
,
2355
(
2010
).
24.
J.-Y.
Kim
,
D.
Jang
, and
J. R.
Greer
,
Int. J. Plast.
28
,
46
(
2012
).
25.
J. R.
Cahoon
,
W. H.
Broughton
, and
A. R.
Kutzak
,
Metall. Trans.
2
,
1979
(
1971
).
26.
Z. C.
Cordero
,
B. E.
Knight
, and
C. A.
Schuh
,
Int. Mater. Rev.
61
,
495
(
2016
).
27.
K. A.
Dahmen
,
Y.
Ben-Zion
, and
J. T.
Uhl
,
Phys. Rev. Lett.
102
,
175501
(
2009
).
28.
G.
Sparks
and
R.
Maaß
,
Phys. Rev. Mater.
2
,
120601
(
2018
).
29.
H.
Van Swygenhoven
,
P. M.
Derlet
, and
A. G.
Frøseth
,
Nat. Mater.
3
,
399
(
2004
).
30.
S.
Kondo
,
T.
Mitsuma
,
N.
Shibata
, and
Y.
Ikuhara
,
Sci. Adv.
2
,
e1501926
(
2016
).
31.
H.
Li
,
S.
Gao
,
Y.
Tomota
,
S.
Ii
,
N.
Tsuji
, and
T.
Ohmura
,
Acta Mater.
206
, 116621, (2021).
33.
J. C.
Li
,
Trans. Metall. Soc. AIME
227
,
239
(
1963
).
34.
J. P.
Hirth
,
Metall. Trans.
3
,
3047
(
1972
).
35.
M. A.
Meyersm
and
E.
Ashworth
,
Philos. Mag. A
46
,
737
(
1982
).
37.
38.
R.
Yuan
,
I. J.
Beyerlein
, and
C.
Zhou
,
Acta Mater.
90
,
169
(
2015
).
39.
J. R.
Greer
,
W. C.
Oliver
, and
W. D.
Nix
,
Acta Mater.
53
,
1821
(
2005
).
40.
S. H.
Oh
,
M.
Legros
,
D.
Kiener
, and
G.
Dehm
,
Nat. Mater.
8
,
95
(
2009
).
41.
D.
Kiener
and
A. M.
Minor
,
Nano Lett.
11
,
3816
(
2011
).
42.
C. P.
Frick
,
B. G.
Clark
,
S.
Orso
,
A. S.
Schneider
, and
E.
Arzt
,
Mater. Sci. Eng. A
489
,
319
(
2008
).
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