In this study, an in situ catalytic radical probe system together with a software platform is developed to measure concentrations of reactive species in low-temperature plasmas with high spatial resolutions. The radical probes can be used to determine radical densities of hydrogen, nitrogen, and oxygen independently, in pairs and often simultaneously in any continuous plasma source in a vacuum environment. The basic principle and advantage of a probe array is the capability to distinguish between different gas species due to several sensitive elements acting as recombination catalysts. Radical densities of hydrogen, nitrogen, and oxygen were measured in a helicon plasma source. Generally, it is observed that radical densities increase with respect to pressure and power. Additionally, the electron density and electron temperature were measured by Langmuir probes. The electron density increased with increasing power and pressure. Electron temperature increased with power but decreased with increasing pressure. The key to getting absolute numbers of radical densities is based on knowing the recombination coefficient of the given gas on the catalytic surface. The probe system measures densities in a broad range of reactive species’ concentrations varying from about 1013 to 1015 cm−3.
Skip Nav Destination
,
,
,
,
,
Article navigation
March 2021
Research Article|
March 03 2021
Radical probe system for in situ measurements of radical densities of hydrogen, oxygen, and nitrogen Available to Purchase
Dren Qerimi;
Dren Qerimi
a)
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
Ivan Shchelkanov;
Ivan Shchelkanov
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
Gianluca Panici;
Gianluca Panici
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
Arihant Jain;
Arihant Jain
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
James Wagner;
James Wagner
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
David N. Ruzic
David N. Ruzic
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801
Search for other works by this author on:
Dren Qerimi
a)
Ivan Shchelkanov
Gianluca Panici
Arihant Jain
James Wagner
David N. Ruzic
Department of Nuclear, Center for Plasma Material Interactions, Plasma and Radiological Engineering, University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801a)
Electronic mail: [email protected]
J. Vac. Sci. Technol. A 39, 023003 (2021)
Article history
Received:
November 17 2020
Accepted:
February 11 2021
Citation
Dren Qerimi, Ivan Shchelkanov, Gianluca Panici, Arihant Jain, James Wagner, David N. Ruzic; Radical probe system for in situ measurements of radical densities of hydrogen, oxygen, and nitrogen. J. Vac. Sci. Technol. A 1 March 2021; 39 (2): 023003. https://doi.org/10.1116/6.0000786
Download citation file:
Pay-Per-View Access
$40.00
Sign In
You could not be signed in. Please check your credentials and make sure you have an active account and try again.
Citing articles via
Perspective on improving the quality of surface and material data analysis in the scientific literature with a focus on x-ray photoelectron spectroscopy (XPS)
George H. Major, Joshua W. Pinder, et al.
Low-resistivity molybdenum obtained by atomic layer deposition
Kees van der Zouw, Bernhard Y. van der Wel, et al.
Machine-learning-enabled on-the-fly analysis of RHEED patterns during thin film deposition by molecular beam epitaxy
Tiffany C. Kaspar, Sarah Akers, et al.
Related Content
Determination of recombination coefficients for hydrogen, oxygen, and nitrogen gasses via in situ radical probe system
J. Vac. Sci. Technol. A (March 2021)
Optical and mass spectrometric measurements of dissociation in low frequency, high density, remote source O2/Ar and NF3/Ar plasmas
J. Vac. Sci. Technol. A (February 2020)
Synergistic interactions of H2 and N2 with molten gallium in the presence of plasma
J. Vac. Sci. Technol. A (December 2017)
The fixed-bias Langmuir probe on the Communication/Navigation Outage Forecast System satellite: Calibration and validation
Rev. Sci. Instrum. (November 2012)
Determination of atomic oxygen density with a nickel catalytic probe
J. Vac. Sci. Technol. A (March 2000)