A direct, noninvasive thermometry method based on the temperature dependence of the in-plane electrical resistance R(T) of 20 nm Pt films on Si-based semiconducting substrates is presented. At the calibration stage, the entire sample is slowly heated or cooled by external means. For moderately doped semiconductors, the R(T) dependence is closely linear at low temperatures (T < 300 K), when the nanofilm metal conductance dominates, followed by a maximum and a subsequent decrease attributed to an increasing substrate conductance at higher temperatures. The position of the maximum depends on the Pt–substrate interface conditions, in particular, on the presence of an oxide layer, and may vary from 350 to 500 K. With the R(T) dependence measured in equilibrium one can derive T(R), which provides a highly accurate method for noninvasive measuring and controlling the temperature of the nanofilm with a direct resistive heating technique. Accuracy of the present method for dynamical measurement is shown to be significantly better than that of a standard approach using a Pt resistance temperature detector attached to the nanofilm for heating rates of 1–7 K/s.
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May 2012
Research Article|
March 28 2012
Noninvasive measurement and control of the temperature of Pt nanofilms on Si supports
I. I. Nedrygailov;
I. I. Nedrygailov
Fakultät für Chemie,
Universität Duisburg-Essen
, D-45117 Essen, Germany
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E. Hasselbrink;
E. Hasselbrink
Fakultät für Chemie,
Universität Duisburg-Essen
, D-45117 Essen, Germany
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D. Diesing;
D. Diesing
a)
Fakultät für Chemie,
Universität Duisburg-Essen
, D-45117 Essen, Germany
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S. K. Dasari;
S. K. Dasari
Department of Civil and Materials Engineering,
University of Illinois
, Chicago, Illinois 60607
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M. A. Hashemian;
M. A. Hashemian
Department of Civil and Materials Engineering,
University of Illinois
, Chicago, Illinois 60607
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E. G. Karpov
E. G. Karpov
Department of Civil and Materials Engineering,
University of Illinois
, Chicago, Illinois 60607
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a)
Author to whom correspondence should be addressed; electronic mail: Detlef.Diesing@Uni-Duisburg-Essen.de
Journal of Vacuum Science & Technology A 30, 030601 (2012)
Article history
Received:
November 02 2011
Accepted:
March 06 2012
Citation
I. I. Nedrygailov, E. Hasselbrink, D. Diesing, S. K. Dasari, M. A. Hashemian, E. G. Karpov; Noninvasive measurement and control of the temperature of Pt nanofilms on Si supports. J. Vac. Sci. Technol. A 1 May 2012; 30 (3): 030601. https://doi.org/10.1116/1.3696973
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