High mobility electron gases confined at material interfaces have been a venue for major discoveries in condensed matter physics. Ultra-high vacuum (UHV) technologies played a key role in creating such high-quality interfaces. The advent of two-dimensional (2D) materials brought new opportunities to explore exotic physics in flat lands. UHV technologies may once again revolutionize research in low dimensions by facilitating the construction of ultra-clean interfaces with a wide variety of 2D materials. Here, we describe the design and operation of a UHV 2D material device fabrication system, in which the entire fabrication process is performed under pressure lower than 5 × 10−10 mbar. Specifically, the UHV system enables the exfoliation of atomically clean 2D materials. Subsequent in situ assembly of van der Waals heterostructures produces high-quality interfaces that are free of contamination. We demonstrate functionalities of this system through exemplary fabrication of various 2D materials and their heterostructures.
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January 2023
Research Article|
January 10 2023
An ultra-high vacuum system for fabricating clean two-dimensional material devices
Shuaifei Guo
;
Shuaifei Guo
(Data curation, Investigation, Methodology, Software, Writing – original draft, Writing – review & editing)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
2
Shanghai Qi Zhi Institute
, Shanghai 200232, China
3
Shanghai Research Center for Quantum Sciences
, Shanghai 201315, China
4
Institute for Nanoelectronic Devices and Quantum Computing, Fudan University
, Shanghai 200433, China
5
Zhangjiang Fudan International Innovation Center, Fudan University
, Shanghai 201210, China
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Mingyan Luo
;
Mingyan Luo
(Data curation, Investigation, Methodology, Software)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
2
Shanghai Qi Zhi Institute
, Shanghai 200232, China
3
Shanghai Research Center for Quantum Sciences
, Shanghai 201315, China
4
Institute for Nanoelectronic Devices and Quantum Computing, Fudan University
, Shanghai 200433, China
5
Zhangjiang Fudan International Innovation Center, Fudan University
, Shanghai 201210, China
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Gang Shi
;
Gang Shi
(Methodology)
6
Department of Physics, Southern University of Science and Technology
, 518055 Shenzhen, China
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Ning Tian;
Ning Tian
(Data curation, Resources)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
2
Shanghai Qi Zhi Institute
, Shanghai 200232, China
3
Shanghai Research Center for Quantum Sciences
, Shanghai 201315, China
4
Institute for Nanoelectronic Devices and Quantum Computing, Fudan University
, Shanghai 200433, China
5
Zhangjiang Fudan International Innovation Center, Fudan University
, Shanghai 201210, China
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Zhe Huang;
Zhe Huang
(Data curation)
7
State Key Laboratory of Functional Materials for Informatics, Shanghai Institute of Microsystem and Information Technology (SIMIT), Chinese Academy of Sciences
, Shanghai 200050, China
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Fangyuan Yang
;
Fangyuan Yang
(Methodology)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
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Liguo Ma
;
Liguo Ma
(Methodology)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
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Nai Zhou Wang
;
Nai Zhou Wang
(Resources)
8
Hefei National Laboratory for Physical Science at Microscale and Department of Physics, University of Science and Technology of China
, Hefei, Anhui 230026, China
9
Key Laboratory of Strongly Coupled Quantum Matter Physics, University of Science and Technology of China
, Hefei, Anhui 230026, China
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Qinzhen Shi
;
Qinzhen Shi
(Software)
10
Center for Biomedical Engineering, Fudan University
, Shanghai 200438, China
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Kailiang Xu
;
Kailiang Xu
(Software)
10
Center for Biomedical Engineering, Fudan University
, Shanghai 200438, China
11
Academy for Engineering and Technology, Fudan University
, Shanghai, China
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Zihan Xu
;
Zihan Xu
(Resources)
12
SixCarbon Technology, Youmagang Industry Park
, Shenzhen 518106, China
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Kenji Watanabe
;
Kenji Watanabe
(Resources)
13
Research Center for Functional Materials, National Institute for Materials Science
, 1-1 Namiki, Tsukuba 305-0044, Japan
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Takashi Taniguchi
;
Takashi Taniguchi
(Resources)
14
International Center for Materials Nanoarchitectonics, National Institute for Materials Science
, 1-1 Namiki, Tsukuba 305-0044, Japan
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Xian Hui Chen
;
Xian Hui Chen
(Resources)
8
Hefei National Laboratory for Physical Science at Microscale and Department of Physics, University of Science and Technology of China
, Hefei, Anhui 230026, China
9
Key Laboratory of Strongly Coupled Quantum Matter Physics, University of Science and Technology of China
, Hefei, Anhui 230026, China
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Dawei Shen
;
Dawei Shen
(Data curation)
7
State Key Laboratory of Functional Materials for Informatics, Shanghai Institute of Microsystem and Information Technology (SIMIT), Chinese Academy of Sciences
, Shanghai 200050, China
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Liyuan Zhang;
Liyuan Zhang
(Methodology)
6
Department of Physics, Southern University of Science and Technology
, 518055 Shenzhen, China
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Wei Ruan
;
Wei Ruan
a)
(Supervision, Writing – original draft, Writing – review & editing)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
3
Shanghai Research Center for Quantum Sciences
, Shanghai 201315, China
4
Institute for Nanoelectronic Devices and Quantum Computing, Fudan University
, Shanghai 200433, China
5
Zhangjiang Fudan International Innovation Center, Fudan University
, Shanghai 201210, China
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Yuanbo Zhang
Yuanbo Zhang
a)
(Conceptualization, Project administration, Visualization, Writing – original draft, Writing – review & editing)
1
State Key Laboratory of Surface Physics and Department of Physics, Fudan University
, Shanghai 200438, China
2
Shanghai Qi Zhi Institute
, Shanghai 200232, China
3
Shanghai Research Center for Quantum Sciences
, Shanghai 201315, China
4
Institute for Nanoelectronic Devices and Quantum Computing, Fudan University
, Shanghai 200433, China
5
Zhangjiang Fudan International Innovation Center, Fudan University
, Shanghai 201210, China
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Rev. Sci. Instrum. 94, 013903 (2023)
Article history
Received:
July 17 2022
Accepted:
December 21 2022
Citation
Shuaifei Guo, Mingyan Luo, Gang Shi, Ning Tian, Zhe Huang, Fangyuan Yang, Liguo Ma, Nai Zhou Wang, Qinzhen Shi, Kailiang Xu, Zihan Xu, Kenji Watanabe, Takashi Taniguchi, Xian Hui Chen, Dawei Shen, Liyuan Zhang, Wei Ruan, Yuanbo Zhang; An ultra-high vacuum system for fabricating clean two-dimensional material devices. Rev. Sci. Instrum. 1 January 2023; 94 (1): 013903. https://doi.org/10.1063/5.0110875
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