We have developed a helium gas flow cryostat for use on synchrotron tender to hard X-ray beamlines. Very efficient sample cooling is achieved because the sample is placed directly in the cooling helium flow on a removable sample holder. The cryostat is compact and easy to operate; samples can be changed in less than 5 min at any temperature. The cryostat has a temperature range of 2.5–325 K with temperature stability better than 0.1 K. The very wide optical angle and the ability to operate in any orientation mean that the cryostat can easily be adapted for different X-ray techniques. It is already in use on different beamlines at the European Synchrotron Radiation Facility (ESRF), ALBA Synchrotron Light Facility (ALBA), and Diamond Light Source (DLS) for inelastic X-ray scattering, powder diffraction, and X-ray absorption spectroscopy. Results obtained at these beamlines are presented here.
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November 2016
Research Article|
November 08 2016
A compact and versatile dynamic flow cryostat for photon science Available to Purchase
Peter J. E. M. van der Linden
;
Peter J. E. M. van der Linden
a)
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
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Marco Moretti Sala;
Marco Moretti Sala
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
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Christian Henriquet;
Christian Henriquet
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
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Matteo Rossi
;
Matteo Rossi
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
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Kenya Ohgushi;
Kenya Ohgushi
2Department of Physics, Graduate School of Science,
Tohoku University
, 6-3, Aramaki Aza-Aoba, Aoba-ku, Sendai, Miyagi 980-8578, Japan
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François Fauth
;
François Fauth
3
ALBA Synchrotron Light Source
, Carretera BP 1413, Km. 3.3, 08290 Cerdanyola del Vallès, Barcelona, Spain
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Laura Simonelli;
Laura Simonelli
3
ALBA Synchrotron Light Source
, Carretera BP 1413, Km. 3.3, 08290 Cerdanyola del Vallès, Barcelona, Spain
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Carlo Marini;
Carlo Marini
3
ALBA Synchrotron Light Source
, Carretera BP 1413, Km. 3.3, 08290 Cerdanyola del Vallès, Barcelona, Spain
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Edmundo Fraga
;
Edmundo Fraga
3
ALBA Synchrotron Light Source
, Carretera BP 1413, Km. 3.3, 08290 Cerdanyola del Vallès, Barcelona, Spain
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Claire Murray;
Claire Murray
4Diamond Light Source Ltd.,
Harwell Science and Innovation Campus
, Didcot, Oxfordshire OX11 0DE, United Kingdom
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Jonathan Potter;
Jonathan Potter
4Diamond Light Source Ltd.,
Harwell Science and Innovation Campus
, Didcot, Oxfordshire OX11 0DE, United Kingdom
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Michael Krisch
Michael Krisch
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
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Peter J. E. M. van der Linden
1,a)
Marco Moretti Sala
1
Christian Henriquet
1
Matteo Rossi
1
Kenya Ohgushi
2
François Fauth
3
Laura Simonelli
3
Carlo Marini
3
Edmundo Fraga
3
Claire Murray
4
Jonathan Potter
4
Michael Krisch
1
1
ESRF-The European Synchrotron
, CS40220, 38043 Grenoble Cedex 9, France
2Department of Physics, Graduate School of Science,
Tohoku University
, 6-3, Aramaki Aza-Aoba, Aoba-ku, Sendai, Miyagi 980-8578, Japan
3
ALBA Synchrotron Light Source
, Carretera BP 1413, Km. 3.3, 08290 Cerdanyola del Vallès, Barcelona, Spain
4Diamond Light Source Ltd.,
Harwell Science and Innovation Campus
, Didcot, Oxfordshire OX11 0DE, United Kingdom
a)
Author to whom correspondence should be addressed. Electronic mail: [email protected]
Rev. Sci. Instrum. 87, 115103 (2016)
Article history
Received:
June 07 2016
Accepted:
October 10 2016
Citation
Peter J. E. M. van der Linden, Marco Moretti Sala, Christian Henriquet, Matteo Rossi, Kenya Ohgushi, François Fauth, Laura Simonelli, Carlo Marini, Edmundo Fraga, Claire Murray, Jonathan Potter, Michael Krisch; A compact and versatile dynamic flow cryostat for photon science. Rev. Sci. Instrum. 1 November 2016; 87 (11): 115103. https://doi.org/10.1063/1.4966270
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