For a successful point-contact spectroscopy (PCS) measurement, metallic tips of proper shape and smoothness are essential to ensure the ballistic nature of a point-contact junction. Until recently, the fabrication of Au tips suitable for use in point-contact spectroscopy has remained more of an art involving a trial and error method rather than an automated scientific process. To address these issues, we have developed a technique with which one can prepare high quality Au tips reproducibly and systematically. It involves an electronic control of the driving voltages used for an electrochemical etching of a gold wire in a HCl-glycerol mixture or a HCl solution. We find that a stopping current, below which the circuit is set to shut off, is a single very important parameter to produce an Au tip of desired shape. We present detailed descriptions for a two-step etching process for Au tips and also test results from PCS measurements using them.
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March 2015
Research Article|
March 06 2015
Two-step fabrication technique of gold tips for use in point-contact spectroscopy Available to Purchase
S. Narasiwodeyar;
S. Narasiwodeyar
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
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M. Dwyer
;
M. Dwyer
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
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M. Liu;
M. Liu
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
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W. K. Park;
W. K. Park
a)
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
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L. H. Greene
L. H. Greene
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
Search for other works by this author on:
S. Narasiwodeyar
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
M. Liu
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
W. K. Park
a)
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
L. H. Greene
Department of Physics and Material Research Laboratory,
University of Illinois at Urbana-Champaign
, Urbana, Illinois 61801, USA
a)
Author to whom correspondence should be addressed. Electronic mail: [email protected]
Rev. Sci. Instrum. 86, 033903 (2015)
Article history
Received:
December 28 2014
Accepted:
February 16 2015
Citation
S. Narasiwodeyar, M. Dwyer, M. Liu, W. K. Park, L. H. Greene; Two-step fabrication technique of gold tips for use in point-contact spectroscopy. Rev. Sci. Instrum. 1 March 2015; 86 (3): 033903. https://doi.org/10.1063/1.4913661
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