A small-angle x-ray scattering (SAXS) system with a vertical layout (V-SAXS) has been designed and constructed for in situ detection on nanostructures, which is well suitable for in situ study on self-assembly of nanoparticles at liquid interface and polymer processing. A steel-tower frame on a reinforced basement is built as the supporting skeleton for scattering beam path and detector platform, ensuring the system a high working stability and a high operating accuracy. A micro-focus x-ray source combining parabolic three-dimensional multi-layer mirror and scatteringless collimation system provides a highly parallel beam, which allows us to detect the very small angle range. With a sample-to-detector distance of 7 m, the largest measurable length scale is 420 nm in real space. With a large sample zone, it is possible to install different experimental setups such as film stretching machine, which makes the system perfect to follow the microstructures evolution of materials during processing. The capability of the V-SAXS on in situ study is tested with a drying experiment of a free latex droplet, which confirms our initial design.
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December 2014
Research Article|
December 10 2014
A small-angle x-ray scattering system with a vertical layout Available to Purchase
Zhen Wang;
Zhen Wang
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Xiaowei Chen;
Xiaowei Chen
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Lingpu Meng;
Lingpu Meng
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Kunpeng Cui;
Kunpeng Cui
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Lihui Wu;
Lihui Wu
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Liangbin Li
Liangbin Li
a)
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
Search for other works by this author on:
Zhen Wang
Xiaowei Chen
Lingpu Meng
Kunpeng Cui
Lihui Wu
Liangbin Li
a)
National Synchrotron Radiation Lab and College of Nuclear Science and Technology, CAS Key Laboratory of Soft Matter Chemistry,
University of Science and Technology of China
, Hefei, China
a)
Author to whom correspondence should be addressed. Electronic mail: [email protected]
Rev. Sci. Instrum. 85, 125110 (2014)
Article history
Received:
September 23 2014
Accepted:
November 26 2014
Citation
Zhen Wang, Xiaowei Chen, Lingpu Meng, Kunpeng Cui, Lihui Wu, Liangbin Li; A small-angle x-ray scattering system with a vertical layout. Rev. Sci. Instrum. 1 December 2014; 85 (12): 125110. https://doi.org/10.1063/1.4903760
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