Two modifications have been made to a miniature ceramic anvil high pressure cell (mCAC) designed for magnetic measurements at pressures up to 12.6 GPa in a commercial superconducting quantum interference (SQUID) magnetometer [N. Tateiwa et al, Rev. Sci. Instrum. 82, 053906 (2011); N. Tateiwa et al, Rev. Sci. Instrum. 83, 053906 (2012)]. Replacing the Cu-Be piston in the former mCAC with a composite piston composed of the Cu-Be and ceramic cylinders reduces the background magnetization significantly smaller at low temperatures, enabling more precise magnetic measurements at low temperatures. A second modification to the mCAC is the utilization of a ceramic anvil with a hollow in the center of the culet surface. High pressures up to 5 GPa were generated with the “cupped ceramic anvil” with the culet size of 1.0 mm.
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April 2013
Brief Report|
April 24 2013
Note: Improved sensitivity of magnetic measurements under high pressure in miniature ceramic anvil cell for a commercial SQUID magnetometer
Naoyuki Tateiwa;
Naoyuki Tateiwa
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
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Yoshinori Haga;
Yoshinori Haga
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
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Tatsuma D. Matsuda;
Tatsuma D. Matsuda
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
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Zachary Fisk;
Zachary Fisk
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
2
University of California
, Irvine, California 92697, USA
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Shugo Ikeda;
Shugo Ikeda
3Graduate School of Material Science,
University of Hyogo
, Koto, Hyogo 678-1297, Japan
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Hisao Kobayashi
Hisao Kobayashi
3Graduate School of Material Science,
University of Hyogo
, Koto, Hyogo 678-1297, Japan
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Rev. Sci. Instrum. 84, 046105 (2013)
Article history
Received:
February 08 2013
Accepted:
April 08 2013
Citation
Naoyuki Tateiwa, Yoshinori Haga, Tatsuma D. Matsuda, Zachary Fisk, Shugo Ikeda, Hisao Kobayashi; Note: Improved sensitivity of magnetic measurements under high pressure in miniature ceramic anvil cell for a commercial SQUID magnetometer. Rev. Sci. Instrum. 1 April 2013; 84 (4): 046105. https://doi.org/10.1063/1.4802832
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