A nuclear magnetic resonance apparatus for experiments in pulsed high magnetic fields is described. The magnetic field pulses created together with various magnet coils determine the requirements such an apparatus has to fulfill to be operated successfully in pulsed fields. Independent of the chosen coil it is desirable to operate the entire experiment at the highest possible bandwidth such that a correspondingly large temporal fraction of the magnetic field pulse can be used to probe a given sample. Our apparatus offers a bandwidth of up to 20 MHz and has been tested successfully at the Hochfeld-Magnetlabor Dresden, even in a very fast dual coil magnet that has produced a peak field of 94.2 T. Using a medium-sized single coil with a significantly slower dependence, it is possible to perform advanced multi-pulse nuclear magnetic resonance experiments. As an example we discuss a Carr-Purcell spin echo sequence at a field of 62 T.
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August 2012
Research Article|
August 23 2012
Nuclear magnetic resonance apparatus for pulsed high magnetic fields
Benno Meier;
Benno Meier
a)
1
University of Leipzig
, Faculty of Physics and Earth Science, Linnéstrasse 5, 04103 Leipzig, Germany
2
Hochfeld-Magnetlabor Dresden
, Helmholtz-Zentrum Dresden-Rossendorf, 01328 Dresden, Germany
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Jonas Kohlrautz;
Jonas Kohlrautz
1
University of Leipzig
, Faculty of Physics and Earth Science, Linnéstrasse 5, 04103 Leipzig, Germany
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Jürgen Haase;
Jürgen Haase
b)
1
University of Leipzig
, Faculty of Physics and Earth Science, Linnéstrasse 5, 04103 Leipzig, Germany
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Marco Braun;
Marco Braun
3
NMR Service GmbH
, Blumenstrae 70, 99092 Erfurt, Germany
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Frederik Wolff-Fabris;
Frederik Wolff-Fabris
2
Hochfeld-Magnetlabor Dresden
, Helmholtz-Zentrum Dresden-Rossendorf, 01328 Dresden, Germany
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Erik Kampert;
Erik Kampert
2
Hochfeld-Magnetlabor Dresden
, Helmholtz-Zentrum Dresden-Rossendorf, 01328 Dresden, Germany
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Thomas Herrmannsdörfer;
Thomas Herrmannsdörfer
2
Hochfeld-Magnetlabor Dresden
, Helmholtz-Zentrum Dresden-Rossendorf, 01328 Dresden, Germany
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Joachim Wosnitza
Joachim Wosnitza
2
Hochfeld-Magnetlabor Dresden
, Helmholtz-Zentrum Dresden-Rossendorf, 01328 Dresden, Germany
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Rev. Sci. Instrum. 83, 083113 (2012)
Article history
Received:
July 06 2012
Accepted:
August 04 2012
Citation
Benno Meier, Jonas Kohlrautz, Jürgen Haase, Marco Braun, Frederik Wolff-Fabris, Erik Kampert, Thomas Herrmannsdörfer, Joachim Wosnitza; Nuclear magnetic resonance apparatus for pulsed high magnetic fields. Rev. Sci. Instrum. 1 August 2012; 83 (8): 083113. https://doi.org/10.1063/1.4746988
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