A miniature ceramic anvil high pressure cell (mCAC) was earlier designed by us for magnetic measurements at pressures up to 7.6 GPa in a commercial superconducting quantum interference magnetometer [N. Tateiwa et al., Rev. Sci. Instrum. 82, 053906 (2011)] https://doi.org/10.1063/1.3590745. Here, we describe methods to generate pressures above 10 GPa in the mCAC. The efficiency of the pressure generation is sharply improved when the Cu-Be gasket is sufficiently preindented. The maximum pressure for the 0.6 mm culet anvils is 12.6 GPa when the Cu-Be gasket is preindented from the initial thickness of 300–60 μm. The 0.5 mm culet anvils were also tested with a rhenium gasket. The maximum pressure attainable in the mCAC is about 13 GPa. The present cell was used to study YbCu2Si2 which shows a pressure induced transition from the non-magnetic to magnetic phases at 8 GPa. We confirm a ferromagnetic transition from the dc magnetization measurement at high pressure. The mCAC can detect the ferromagnetic ordered state whose spontaneous magnetic moment is smaller than 1 μB per unit cell. The high sensitivity for magnetic measurements in the mCAC may result from the simplicity of cell structure. The present study shows the availability of the mCAC for precise magnetic measurements at pressures above 10 GPa.
Skip Nav Destination
Article navigation
May 2012
Research Article|
May 31 2012
Magnetic measurements at pressures above 10 GPa in a miniature ceramic anvil cell for a superconducting quantum interference device magnetometer
Naoyuki Tateiwa;
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
Search for other works by this author on:
Yoshinori Haga;
Yoshinori Haga
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
2JST,
Transformative Research-Project on Iron Pnictides (TRIP)
, Tokyo 102-0075, Japan
Search for other works by this author on:
Tatsuma D. Matsuda;
Tatsuma D. Matsuda
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
Search for other works by this author on:
Zachary Fisk
Zachary Fisk
1Advanced Science Research Center,
Japan Atomic Energy Agency
, Tokai, Naka, Ibaraki 319-1195, Japan
3
University of California
, Irvine, California 92697, USA
Search for other works by this author on:
a)
Electronic mail: tateiwa.naoyuki@jaea.go.jp.
Rev. Sci. Instrum. 83, 053906 (2012)
Article history
Received:
January 25 2012
Accepted:
May 11 2012
Citation
Naoyuki Tateiwa, Yoshinori Haga, Tatsuma D. Matsuda, Zachary Fisk; Magnetic measurements at pressures above 10 GPa in a miniature ceramic anvil cell for a superconducting quantum interference device magnetometer. Rev. Sci. Instrum. 1 May 2012; 83 (5): 053906. https://doi.org/10.1063/1.4722945
Download citation file:
Sign in
Don't already have an account? Register
Sign In
You could not be signed in. Please check your credentials and make sure you have an active account and try again.
Pay-Per-View Access
$40.00
Citing articles via
Overview of the early campaign diagnostics for the SPARC tokamak (invited)
M. L. Reinke, I. Abramovic, et al.
Uniform microwave field formation for control of ensembles of negatively charged nitrogen vacancy in diamond
Oleg Rezinkin, Marina Rezinkina, et al.
An instrumentation guide to measuring thermal conductivity using frequency domain thermoreflectance (FDTR)
Dylan J. Kirsch, Joshua Martin, et al.
Related Content
Note: Improved sensitivity of magnetic measurements under high pressure in miniature ceramic anvil cell for a commercial SQUID magnetometer
Rev. Sci. Instrum. (April 2013)
Miniature ceramic-anvil high-pressure cell for magnetic measurements in a commercial superconducting quantum interference device magnetometer
Rev. Sci. Instrum. (May 2011)
Review of modern instrumentation for magnetic measurements at high pressure and low temperature
Low Temp. Phys. (August 2014)
Study on preparation of Luffa activated carbon and its adsorption of metal ions
AIP Conference Proceedings (March 2017)