We report the design of an optical floating-zone furnace for single-crystal growth under ultra-high vacuum (UHV) compatible conditions. The system is based on a commercial image furnace, which has been refurbished to be all-metal sealed. Major changes concern the use of UHV rotary feedthroughs and bespoke quartz-metal seals with metal-O-rings at the lamp stage. As a consequence, the procedure of assembling the furnace for crystal growth is changed completely. Bespoke heating jackets permit to bake the system. For compounds with elevated vapor pressures, the ultra-high vacuum serves as a precondition for the use of a high-purity argon atmosphere up to 10 bar. In the ferromagnetic Heusler compound Cu
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January 2011
Research Article|
January 14 2011
Ultra-high vacuum compatible image furnace
A. Neubauer;
A. Neubauer
1Physik-Department E21,
Technische Universität München
, D-85748 Garching, Germany
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J. Bœuf;
J. Bœuf
2Physikalisches Institut,
Karlsruher Institut für Technologie
, D-76128 Karlsruhe, Germany
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A. Bauer;
A. Bauer
1Physik-Department E21,
Technische Universität München
, D-85748 Garching, Germany
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B. Russ;
B. Russ
1Physik-Department E21,
Technische Universität München
, D-85748 Garching, Germany
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H. v. Löhneysen;
H. v. Löhneysen
2Physikalisches Institut,
Karlsruher Institut für Technologie
, D-76128 Karlsruhe, Germany
3Institut für Festkörperphysik,
Karlsruher Institut für Technologie
, D-76021 Karlsruhe, Germany
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C. Pfleiderer
C. Pfleiderer
a)
1Physik-Department E21,
Technische Universität München
, D-85748 Garching, Germany
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a)
Electronic mail: christian.pfleiderer@frm2.tum.de.
Rev. Sci. Instrum. 82, 013902 (2011)
Article history
Received:
July 27 2010
Accepted:
November 10 2010
Citation
A. Neubauer, J. Bœuf, A. Bauer, B. Russ, H. v. Löhneysen, C. Pfleiderer; Ultra-high vacuum compatible image furnace. Rev. Sci. Instrum. 1 January 2011; 82 (1): 013902. https://doi.org/10.1063/1.3523056
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