Spot profile analysis low energy electron diffraction (SPA-LEED) is one of the most versatile and powerful methods for the determination of the structure and morphology of surfaces even at elevated temperatures. In setups where the sample is heated directly by an electric current, the resolution of the diffraction images at higher temperatures can be heavily degraded due to the inhomogeneous electric and magnetic fields around the sample. Here we present an easily applicable modification of the common data acquisition hardware of the SPA-LEED, which enables the system to work in a pulsed heating mode: Instead of heating the sample with a constant current, a square wave is used and electron counting is only performed when the current through the sample vanishes. Thus, undistorted diffration images can be acquired at high temperatures.
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November 2004
Research Article|
November 01 2004
Chopped sample heating for quantitative profile analysis of low energy electron diffraction spots at high temperatures
P. Kury;
P. Kury
Institut für Laser- und Plasmaphysik, Universität Duisburg-Essen, D-45117 Essen, Germany
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P. Zahl;
P. Zahl
Institut für Laser- und Plasmaphysik, Universität Duisburg-Essen, D-45117 Essen, Germany
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M. Horn-von Hoegen;
M. Horn-von Hoegen
Institut für Laser- und Plasmaphysik, Universität Duisburg-Essen, D-45117 Essen, Germany
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C. Voges;
C. Voges
Institut für Festkörperphysik, Abt. Oberflächen, Universität Hannover, D-30167 Hannover, Germany
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H. Frischat;
H. Frischat
Institut für Festkörperphysik, Abt. Oberflächen, Universität Hannover, D-30167 Hannover, Germany
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H.-L. Günter;
H.-L. Günter
Institut für Festkörperphysik, Abt. Oberflächen, Universität Hannover, D-30167 Hannover, Germany
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H. Pfnür;
H. Pfnür
Institut für Festkörperphysik, Abt. Oberflächen, Universität Hannover, D-30167 Hannover, Germany
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M. Henzler
M. Henzler
Institut für Festkörperphysik, Abt. Oberflächen, Universität Hannover, D-30167 Hannover, Germany
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Rev. Sci. Instrum. 75, 4911–4915 (2004)
Article history
Received:
January 22 2004
Accepted:
July 06 2004
Citation
P. Kury, P. Zahl, M. Horn-von Hoegen, C. Voges, H. Frischat, H.-L. Günter, H. Pfnür, M. Henzler; Chopped sample heating for quantitative profile analysis of low energy electron diffraction spots at high temperatures. Rev. Sci. Instrum. 1 November 2004; 75 (11): 4911–4915. https://doi.org/10.1063/1.1807003
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