Synthetic diamond has been successfully used as a backing-plate in the diamond-anvil cell up to 223 GPa. Use of diamond for the backing-plate has a great advantage for powder x-ray diffraction experiments at ultrahigh pressures, for it makes it possible to measure full Debye–Scherrer rings to a maximum scattering angle of The mechanical strength of the diamond backing-plate should contribute to the extension of the current pressure limit of the diamond-anvil cell. Problems and future improvements of the design are discussed.
REFERENCES
1.
2.
3.
R.
LeToullec
, P.
Loubeyre
, J. P.
Pinceaux
, H. K.
Mao
, and J.
Hu
, High Press. Res.
6
, 379
(1992
).4.
P.
Loubeyre
, R.
LeToullec
, D.
Hausermann
, M.
Hanfland
, R. J.
Hemley
, H. K.
Mao
, and L. W.
Finger
, Nature (London)
383
, 702
(1996
).5.
6.
T.
Yamanaka
, T.
Fukuda
, T.
Hattori
, and H.
Sumiya
, Rev. Sci. Instrum.
72
, 1458
(2001
).7.
R. J.
Hemley
, A. P.
Jephcoat
, H. K.
Mao
, L. C.
Ming
, and M. H.
Manghnani
, Nature (London)
334
, 52
(1988
).8.
K. J.
Kingma
, C.
Meade
, R. J.
Hemley
, H.-k.
Mao
, and D. R.
Veblen
, Science
259
, 666
(1993
).9.
J.
Haines
, J. M.
Léger
, F.
Gorelli
, and M.
Hanfland
, Phys. Rev. Lett.
87
, 155503
(2001
).10.
11.
12.
S. Nakano and K. Takemura (unpublished).
13.
K.
Takemura
, O.
Shimomura
, and H.
Fujihisa
, Phys. Rev. Lett.
66
, 2014
(1991
).14.
K.
Takemura
, N. E.
Christensen
, D. L.
Novikov
, K.
Syassen
, U.
Schwarz
, and M.
Hanfland
, Phys. Rev. B
61
, 14399
(2000
).15.
N. C.
Holmes
, J. A.
Moriarty
, G. R.
Gathers
, and W. J.
Nellis
, J. Appl. Phys.
66
, 2962
(1989
).16.
In another experiment with the mount hemisphere with a 5 mm top hole, we have successfully measured the full Debye–Scherrer rings up to in 2θ at 152 GPa.
17.
H.
Sumiya
, N.
Toda
, Y.
Nishibayashi
, and S.
Satoh
, J. Cryst. Growth
178
, 485
(1997
).18.
M.
Baggen
, R.
Manuputy
, R.
Scheltema
, and A.
Lagendijk
, Rev. Sci. Instrum.
59
, 2592
(1988
).19.
A.
Dadashev
, M. P.
Pasternak
, G. Kh.
Rozenberg
, and R. D.
Taylor
, Rev. Sci. Instrum.
72
, 2633
(2001
).20.
This content is only available via PDF.
© 2003 American Institute of Physics.
2003
American Institute of Physics
You do not currently have access to this content.