A force sensor based on a fiber-optic interferometric displacement transducer incorporated in an ultrahigh vacuum atomic force microscope is described. The operation of the sensor is based on balancing the tip-sample interfacial force using an electrostatic actuator. The electrodes of the actuator are formed by the grounded W cantilever and the metallized end facet of the optical fiber used by the interferometer. Chemical reduction of Ag by a wet chemical method is used for metal coating of the fiber end. A special masking procedure is used to obtain a window hole in the metal coating at the position of the fiber core to allow for optical beam output. Using a window instead of a semitransparent metal film allows us to save the low-finesse characteristics of the interferometer which facilitates the calibration of cantilever displacement. The performance of the sensor is discussed and exemplified by experimental results from force-separation measurements on the W–Au system in ultrahigh vacuum.

1.
G.
Binnig
,
C. F.
Quate
, and
Ch.
Gerber
,
Phys. Rev. Lett.
56
,
930
(
1986
).
2.
N. A.
Burnham
,
R. J.
Colton
, and
H. M.
Pollock
,
Nanotechnology
4
,
64
(
1993
).
3.
A.
Stalder
and
U.
Dürig
,
Probe Microscopy
1
,
135
(
1998
).
4.
S. A.
Joyce
and
J. E.
Houston
,
Rev. Sci. Instrum.
62
,
710
(
1991
).
5.
G. L.
Miller
,
J. E.
Griffith
,
E. R.
Wagner
, and
D. A.
Grigg
,
Rev. Sci. Instrum.
62
,
705
(
1991
).
6.
B.
Gauthier-Manuel
,
Europhys. Lett.
17
,
195
(
1992
).
7.
A. M.
Stewart
and
J. L.
Parker
,
Rev. Sci. Instrum.
63
,
5626
(
1992
).
8.
S. P.
Jarvis
,
U.
Dürig
,
M. A.
Lantz
,
H.
Yamada
, and
H.
Tokumoto
,
Appl. Phys. A: Mater. Sci. Process.
66
,
S211
(
1998
).
9.
N.
Kato
,
H.
Kikuta
,
T.
Nakano
,
T.
Matsumoto
, and
K.
Iwata
,
Rev. Sci. Instrum.
70
,
2402
(
1999
).
10.
M. R.
Sørensen
,
M.
Brandbyge
, and
K. W.
Jacobsen
,
Phys. Rev. B
57
,
3283
(
1998
).
11.
S. M.
Lindsay
,
Y. L.
Lyubchenko
,
N. J.
Tao
,
Y. Q.
Li
,
P. I.
Oden
,
J. A.
DeRose
, and
J.
Pan
,
J. Vac. Sci. Technol. A
11
,
808
(
1993
).
12.
S.
Yamamoto
,
H.
Yamada
, and
H.
Tokumoto
,
Rev. Sci. Instrum.
68
,
4132
(
1997
).
13.
N.
Kato
,
I.
Suzuki
,
H.
Kikuta
, and
K.
Iwata
,
Rev. Sci. Instrum.
66
,
5532
(
1995
).
14.
N.
Kato
,
I.
Suzuki
,
H.
Kikuta
, and
K.
Iwata
,
Rev. Sci. Instrum.
68
,
2475
(
1997
).
15.
J.
Mertz
,
O.
Marti
, and
J.
Mlynek
,
Appl. Phys. Lett.
62
,
2344
(
1993
).
16.
T.
Aoki
,
M.
Hiroshima
,
K.
Kitamura
,
M.
Tokunaga
, and
T.
Yananida
,
Ultramicroscopy
70
,
45
(
1997
).
17.
P. J.
Bryant
,
H. S.
Kim
,
R. H.
Deeken
, and
Y. C.
Cheng
,
J. Vac. Sci. Technol. A
8
,
3502
(
1990
).
18.
D.
Rugar
,
H. J.
Mamin
, and
P.
Guethner
,
Appl. Phys. Lett.
55
,
2588
(
1989
).
19.
L.
Olsson
,
R.
Wigren
, and
R.
Erlandsson
,
Rev. Sci. Instrum.
67
,
2289
(
1996
).
20.
W. R. Smythe, S. Silver, J. R. Whinnery, and D. J. Angelakos, American Institute of Physics Handbook (McGraw-Hill, New York, 1963).
21.
R.
Erlandsson
and
L.
Olsson
,
Rev. Sci. Instrum.
67
,
1472
(
1996
).
22.
J. P.
Cleveland
,
S.
Manne
,
O.
Bocek
, and
P. K.
Hansma
,
Rev. Sci. Instrum.
64
,
403
(
1993
).
23.
P. J.
Mulhern
,
T.
Hubbard
,
C. S.
Arnold
,
B. L.
Blackford
, and
M. H.
Jericho
,
Rev. Sci. Instrum.
62
,
1280
(
1991
).
24.
Metal Finishing, 66th Guidebook and Directory Issue (Westwood, NJ, 1998), Vol. 95, p. 381.
25.
Etching was done with a mixture of CrO3/H2SO4 with a weight ratio of 0.4:1 for 1 h. This was followed by neutralization in a 0.6% solution of Na2S2O5 for 30 min. Sensitizing was done with a 10% solution of SnCl2 for 10 min. Solution for Ag reduction consists of two parts—Part A: AgNO3/KOH/H2O (5 g/2.5 g/100 ml) and Part B (boiled and cooled before using): Sugar/HNO3/H2O (45 g/2 ml/500 ml). Metallizing was done in a mixture of Part A/Part B in a ratio of 4:1 (mixed immediately before using) for 50 s. All stages were followed by rinsing and performed at room temperature.
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