The orientation dependence of thin-crystal lattice fringes can be gracefully quantified using fringe-visibility maps, a direct-space analog of Kikuchi maps [Nishikawa and Kikuchi, Nature (London)121, 1019 (1928)]. As in navigation of reciprocal space with the aid of Kikuchi lines, fringe-visibility maps facilitate acquisition of crystallographic information from lattice images. In particular, these maps can help researchers to determine the three-dimensional lattice of individual nanocrystals, to “fringe-fingerprint” collections of randomly oriented particles, and to measure local specimen thickness with only a modest tilt. Since the number of fringes in an image increases with maximum spatial-frequency squared, these strategies (with help from more precise goniometers) will be more useful as aberration correction moves resolutions into the subangstrom range.

1.
H.
Kung
and
T.
Foecke
,
MRS Bull.
24
,
14
(
1999
).
2.
W. A.
Jesser
,
G.
Shiflet
,
G.
Allen
, and
J.
Crawford
,
Mater. Res. Innovations
2
,
211
(
1999
).
3.
M.
Wautelet
,
Nanotechnology
3
,
42
(
1992
).
4.
M.
Wautelet
,
Nanotechnology
12
,
68
(
2001
).
5.
W. M.
Tolles
,
MRS Bull.
25
,
36
(
2000
).
6.
P.
Fraundorf
,
Ultramicroscopy
22
,
225
(
1987
).
7.
R.
Henderson
and
P. N. T.
Unwin
,
Nature (London)
257
,
28
(
1975
).
8.
R. P.
Goehner
and
P.
Rao
,
Metallography
10
,
415
(
1977
).
9.
R.
Bonnet
,
J. Microsc. Spectrosc. Electron.
3
,
77
(
1978
).
10.
K. -X.
Guo
,
Acta Phys. Sin.
27
,
160
(
1978
).
11.
P.
Fraundorf
,
Ultramicroscopy
6
,
227
(
1981
).
12.
P.
Fraundorf
,
Ultramicroscopy
7
,
203
(
1981
).
13.
J. M.
Cowley
,
J. Electron Microsc.
45
,
3
(
1996
).
14.
P.
Tambuyser
,
J. Mater. Sci. Lett.
3
,
184
(
1984
).
15.
Q.
Liu
,
Micron Microsc. Acta
20
,
261
(
1989
).
16.
Q.
Liu
,
Q. -C.
Meng
, and
B.
Hong
,
Micron Microsc. Acta
20
,
255
(
1989
).
17.
Q.
Liu
,
Micron Microsc. Acta
21
,
105
(
1990
).
18.
P.
Möck
,
Cryst. Res. Technol.
26
,
653
(
1991
).
19.
P.
Möck
,
Cryst. Res. Technol.
26
,
797
(
1991
).
20.
Q.
Liu
,
X.
Huang
, and
M.
Yao
,
Ultramicroscopy
41
,
317
(
1992
).
21.
P.
Moeck
and
W.
Hoppe
,
Tenth European Congress on Electron Microscopy
(
Universidad de Grenada
, Spain,
1992
), Vol.
1
, pp.
193
194
.
22.
Z. S.
Basinski
,
Proceedings of the Fifth International Congress for Electron Microscopy
(
Academic
, New York,
1962
), Vol.
1
, p.
B13
.
23.
D. J.
DeRosier
and
A.
Klug
,
Nature (London)
217
,
130
(
1968
).
24.
J. M.
Cowley
,
Ultramicroscopy
7
,
19
(
1981
).
25.
L. A.
Amos
,
R.
Henderson
, and
P. N. T.
Unwin
,
Prog. Biophys. Mol. Biol.
39
,
183
(
1982
).
26.
A. V.
Crewe
and
D. A.
Crewe
,
Ultramicroscopy
16
,
33
(
1985
).
27.
J.
Frank
and
M.
Radermacher
, in
Advanced Techniques in Biological Electron Microscopy
, edited by
J. K.
Koehler
(
Springer-Verlag
, Berlin,
1986
), Vol.
II
, pp.
1
72
.
28.
H. R.
Wenk
,
K. H.
Downing
,
H.
Meisheng
, and
M. A.
O’Keefe
,
Acta Crystallogr., Sect. A: Found. Crystallogr.
48
,
700
(
1992
).
29.
J.
Frank
and
M.
Rademacher
,
Ultramicroscopy
46
,
241
(
1992
).
30.
J. R.
Jinschek
,
H. A.
Calderon
,
K. J.
Batenburg
,
V.
Radmilovic
, and
C.
Kisielowski
,
Mater. Res. Soc. Symp. Proc.
839
,
P4
5
(
2005
).
31.
W.
Qin
and
P.
Fraundorf
,
Ultramicroscopy
94
,
245
(
2003
).
32.
S.
Nishikawa
and
S.
Kikuchi
,
Nature (London)
121
,
1019
(
1928
).
33.
P.
Hirsch
,
A.
Howie
,
R. B.
Nicholson
,
D. W.
Pashley
, and
M. J.
Whelan
,
Electron Microscopy of Thin Crystals
, 2nd ed. (
Robert E. Krieger
, Huntington, New York,
1977
).
34.
L.
Reimer
,
Transmission Electron Microscopy: Physics of Image Formation and Microanalysis
, 4th ed. (
Springer
, Berlin,
1997
).
35.
D. C.
Joy
, in
Quantitative Scanning Electron Microscopy
, edited by
D. B.
Holt
,
M. D.
Muir
,
L. M.
Boswarva
, and
P. R.
Grant
(
Academic
, New York,
1974
).
36.
J. A.
Venables
and
C. J.
Harland
,
Philos. Mag.
27
,
1193
(
1973
).
37.
M. D.
Graef
,
Introduction to Conventional Transmission Electron Microscopy
(
Cambridge University Press
, Cambridge,
2003
).
38.
P. P.
Ewald
,
Ann. Phys.
54
,
519
(
1917
).
39.
M.
Haider
,
S.
Uhlermann
,
E.
Schwan
,
H.
Rose
,
B.
Kabius
, and
K.
Urban
,
Nature (London)
392
,
768
(
1998
).
40.
P.
Nellist
and
S. J.
Pennycook
,
Phys. Rev. Lett.
81
,
4156
(
1998
).
41.
S. V.
Aert
,
A. J.
den Decker
, and
D. V.
Dyck
,
Micron
35
,
425
(
2004
).
42.
P.
Moeck
,
W.
Qin
, and
P.
Fraundorf
,
Mater. Res. Soc. Symp. Proc.
818
,
Mll
3
(
2004
).
43.
P.
Fraundorf
,
Geochim. Cosmochim. Acta
45
,
915
(
1981
).
44.
P.
Fraundorf
,
E.
Mandell
,
W.
Qin
, and
K.
Chop
, in
Microscopy and Microanalysis
10
, Supplement 2 (
Cambridge University Press
,
2004
), pp.
1262
1263
.
45.
E.
Mandell
,
P.
Fraundorf
, and
M. F.
Bertino
, in
Microscopy and Microanalysis
10
, Supplement 2 (
Cambridge University Press
,
2004
), pp.
1254
1255
.
46.
P. M.
Voyles
,
J. M.
Gibson
, and
M. M. J.
Treacy
,
J. Electron Microsc.
49
,
259
(
2000
).
47.
J. M.
Gibson
and
M. M. J.
Treacy
,
Phys. Rev. Lett.
78
,
1074
(
1997
).
48.
J.
Biskupek
,
U.
Kaiser
, and
A.
Chuvilin
,
Microsc. Microanal.
9
,
166
(
2003
).
49.
B. E.
Warren
,
Phys. Rev.
59
,
693
(
1941
).
50.
L. D.
Marks
,
Ultramicroscopy
12
,
237
(
1983
).
51.
J. C. H.
Spence
,
Experimental High-Resolution Electron Microscopy
, 2nd ed. (
Oxford University Press
, Oxford,
1988
).
52.
J. -O.
Malm
and
M. A.
O’Keefe
,
Ultramicroscopy
68
,
13
(
1997
).
53.
H.
Kohno
,
N.
Ozaki
,
H.
Yoshida
,
K.
Tanaka
, and
S.
Takeda
,
Cryst. Res. Technol.
38
,
1082
(
2003
).
54.
P.
Debye
and
P.
Scherrer
,
Nachr. Ges. Wiss. Goettingen, Math.-Phys. Kl.
1916
,
1
.
55.
A. L.
Patterson
,
Phys. Rev.
56
,
978
(
1939
).
56.
B. E.
Warren
,
X-ray Diffraction
(
Dover
, New York,
1969
).
57.
W.
Qin
, Ph.D. thesis,
University of Missouri - St. Louis/Rolla
,
2000
.
58.
W.
Qin
and
P.
Fraundorf
, in
Microscopy and Microanalysis
6
, Supplement 2 (
Springer
, New York,
2000
), pp.
1040
1041
.
59.
J.
Bailey
, UM-St. Louis Scanned Tip and Electron Image Lab Undergrad Student Project Report No. 10512,
2001
(unpublished).
60.
A. L.
Patterson
,
Phys. Rev.
56
,
972
(
1939
).
61.
A. L. G.
Rees
and
J. A.
Spink
,
Acta Crystallogr.
3
,
316
(
1950
).
62.
H.
Hashimoto
,
A.
Howie
, and
M. J.
Whelan
,
Proc. R. Soc. London, Ser. A
269
,
80
(
1962
).
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