A novel methodology for measuring gas flow from small orifices or nozzles into vacuum is presented. It utilizes a high-intensity femtosecond laser pulse to create a plasma within the gas plume produced by the nozzle, which is imaged by a microscope. Calibration of the imaging system allows for the extraction of absolute number densities. We show detection down to helium densities of cm−3 with a spatial resolution of a few micrometers. The technique is used to characterize the gas flow from a convergent-nozzle aerosol injector [Kirian et al., Struct. Dyn. 2, 041717 (2015)] as used in single-particle diffractive imaging experiments at free-electron laser sources. Based on the measured gas-density profile, we estimate the scattering background signal under typical operating conditions of single-particle imaging experiments and estimate that fewer than 50 photons per shot can be expected on the detector.
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28 March 2017
Research Article|
March 27 2017
Characterizing gas flow from aerosol particle injectors
Daniel A. Horke
;
Daniel A. Horke
a)
1
Center for Free-Electron Laser Science
, DESY, Notkestrasse 85, 22607 Hamburg, Germany
2The Hamburg Center for Ultrafast Imaging,
Universität Hamburg
, Luruper Chaussee 149, 22761 Hamburg, Germany
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Nils Roth
;
Nils Roth
1
Center for Free-Electron Laser Science
, DESY, Notkestrasse 85, 22607 Hamburg, Germany
3Department of Physics,
Universität Hamburg
, Luruper Chaussee 149, 22761 Hamburg, Germany
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Lena Worbs;
Lena Worbs
1
Center for Free-Electron Laser Science
, DESY, Notkestrasse 85, 22607 Hamburg, Germany
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Jochen Küpper
Jochen Küpper
1
Center for Free-Electron Laser Science
, DESY, Notkestrasse 85, 22607 Hamburg, Germany
2The Hamburg Center for Ultrafast Imaging,
Universität Hamburg
, Luruper Chaussee 149, 22761 Hamburg, Germany
3Department of Physics,
Universität Hamburg
, Luruper Chaussee 149, 22761 Hamburg, Germany
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J. Appl. Phys. 121, 123106 (2017)
Article history
Received:
November 16 2016
Accepted:
March 06 2017
Citation
Daniel A. Horke, Nils Roth, Lena Worbs, Jochen Küpper; Characterizing gas flow from aerosol particle injectors. J. Appl. Phys. 28 March 2017; 121 (12): 123106. https://doi.org/10.1063/1.4978914
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