The crystal quality of bulk GaN crystals is continuously improving due to advances in GaN growth techniques. Defect characterization of the GaN substrates by conventional methods is impeded by the very low dislocation density and a large scale defect analysis method is needed. White beam synchrotron radiation x-ray topography (SR-XRT) is a rapid and non-destructive technique for dislocation analysis on a large scale. In this study, the defect structure of an ammonothermal c-plane GaN substrate was recorded using SR-XRT and the image contrast caused by the dislocation induced microstrain was simulated. The simulations and experimental observations agree excellently and the SR-XRT image contrasts of mixed and screw dislocations were determined. Apart from a few exceptions, defect selective etching measurements were shown to correspond one to one with the SR-XRT results.
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28 August 2014
Research Article|
August 25 2014
Synchrotron radiation x-ray topography and defect selective etching analysis of threading dislocations in GaN
Sakari Sintonen;
Sakari Sintonen
a)
1Department of Micro- and Nanosciences,
Aalto University School of Electrical Engineering
, 02150 Espoo, Finland
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Mariusz Rudziński;
Mariusz Rudziński
2Epitaxy Department,
Institute of Electronic Materials Technology
, 01-919 Warsaw, Poland
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Sami Suihkonen;
Sami Suihkonen
1Department of Micro- and Nanosciences,
Aalto University School of Electrical Engineering
, 02150 Espoo, Finland
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Henri Jussila;
Henri Jussila
1Department of Micro- and Nanosciences,
Aalto University School of Electrical Engineering
, 02150 Espoo, Finland
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Michael Knetzger;
Michael Knetzger
3
Fraunhofer Institute for Integrated Systems and Device Technology
, 91058 Erlangen, Germany
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Elke Meissner;
Elke Meissner
3
Fraunhofer Institute for Integrated Systems and Device Technology
, 91058 Erlangen, Germany
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Andreas Danilewsky;
Andreas Danilewsky
4Kristallographie Institut für Geo- und Umweltnaturwissenschaften,
Albert-Ludwigs-Universität Freiburg
, 79104 Freiburg, Germany
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Turkka O. Tuomi;
Turkka O. Tuomi
1Department of Micro- and Nanosciences,
Aalto University School of Electrical Engineering
, 02150 Espoo, Finland
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Harri Lipsanen
Harri Lipsanen
1Department of Micro- and Nanosciences,
Aalto University School of Electrical Engineering
, 02150 Espoo, Finland
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J. Appl. Phys. 116, 083504 (2014)
Article history
Received:
June 09 2014
Accepted:
August 13 2014
Citation
Sakari Sintonen, Mariusz Rudziński, Sami Suihkonen, Henri Jussila, Michael Knetzger, Elke Meissner, Andreas Danilewsky, Turkka O. Tuomi, Harri Lipsanen; Synchrotron radiation x-ray topography and defect selective etching analysis of threading dislocations in GaN. J. Appl. Phys. 28 August 2014; 116 (8): 083504. https://doi.org/10.1063/1.4893901
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