We performed single crystal structure analysis of Sm2Fe17N3 using X-ray diffraction. A pick-up system combined with a micromanipulation tool driven by piezoelectric actuators and a microgripper was used. A single Sm2Fe17Nx particle with the diameter of about 20 μm was picked up, and X-ray diffraction was measured using an X-ray diffractometer at the synchrotron radiation beamline at the Photon Factory, KEK. Single crystal structure analysis of a Sm2Fe17N3 particle was performed and the structure was successfully determined from X-ray diffraction patterns. The space group and the lattice constants were determined to be R-3m (#166) a = b = 8.7206 Å and c = 12.6345 Å, respectively. Atomic positions of Sm and Fe atoms were accurately determined by single crystal structure analysis of only one particle.
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7 May 2014
PROCEEDINGS OF THE 55TH ANNUAL CONFERENCE ON MAGNETISM AND MAGNETIC MATERIALS
14-18 November 2010
Atlanta, Georgia
Research Article|
Magnetism and Magnetic Materials|
January 27 2014
Single crystal structure analysis of a single Sm2Fe17N3 particle
Nobuhito Inami;
Nobuhito Inami
a)
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Yasuo Takeichi;
Yasuo Takeichi
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Tetsuro Ueno;
Tetsuro Ueno
2
National Institute for Materials Science (NIMS)
, Tsukuba 305-0047, Japan
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Kotaro Saito;
Kotaro Saito
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Ryoko Sagayama;
Ryoko Sagayama
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Reiji Kumai;
Reiji Kumai
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Kanta Ono
Kanta Ono
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
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Nobuhito Inami
1,a)
Yasuo Takeichi
1
Tetsuro Ueno
2
Kotaro Saito
1
Ryoko Sagayama
1
Reiji Kumai
1
Kanta Ono
1
1
High Energy Accelerator Research Organization (KEK)
, Tsukuba 305-0801, Japan
2
National Institute for Materials Science (NIMS)
, Tsukuba 305-0047, Japan
a)
Author to whom correspondence should be addressed. Electronic mail: [email protected].
J. Appl. Phys. 115, 17A712 (2014)
Article history
Received:
September 23 2013
Accepted:
October 28 2013
Citation
Nobuhito Inami, Yasuo Takeichi, Tetsuro Ueno, Kotaro Saito, Ryoko Sagayama, Reiji Kumai, Kanta Ono; Single crystal structure analysis of a single Sm2Fe17N3 particle. J. Appl. Phys. 7 May 2014; 115 (17): 17A712. https://doi.org/10.1063/1.4862939
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