Geothermal silica denotes as a potential source of silica for several purposes. One of them stands for silica aerogel. Preparing silica aerogel from leached geothermal silica must be brought into sol gel process. This paper observes the effect of acids concentration, kind of acids solution, and temperature in gelation process by statistical method. Responses were recorded as density, yield quantity, and acid volume. All data was processed by using Design Expert 8.0.6 to optimize operation condition. The result shows that optimum condition can be achieved by using sulfuric acid at 1.8 N and temperature of 56 °C. With these conditions, the gelation product of sodium silicate acquired density of 1.1 g/mL and gel yield of 76.3 g for each of 20 mL of sodium silicate used in gelation.

1.
M. T.
Nayak
,
J. A. E.
Desa
,
V. R.
Reddy
,
C.
Nayak
,
D.
Bhattacharyya
, and
S. N.
Jha
,
J. Non-Cryst. Solids
509
,
42
47
(
2019
).
2.
D. B. v. d.
Heuvel
,
E.
Gunnlaugsson
,
I.
Gunnarsson
,
T. M.
Stawski
,
C. L.
Peacock
, and
L. G.
Benning
,
Geothermics
76
,
231
241
(
2018
).
3.
M.
Stapleton
,
Scaling and Corrosion in Geothermal Operation
(
PowerChem Technology
,
Nevada
,
2002
).
4.
J. E.
Shelby
,
Introduction to glass science and technology
(
The Royal Society of Chemistry
,
2005
), pp.
81
82
.
5.
M.
Khalifa
,
M.
Hajji
, and
H.
Ezzaouia
, “
Impurity removal process for high-purity silica production by acid leaching
” in
First Euro Mediterranean Meeting on Functionalized Materials
,
EPJ Web of Conferences
29
(Sousse,
2012
), pp.
00014
.
6.
A. P.
Rao
,
A.V.
Rao
, and
G. M.
Pajonk
,
Appl. Surf. Sci.
253
,
6032
6040
(
2007
).
7.
A.
Lamy-Mendes
,
R. F.
Silva
, and
L.
Duraes
,
J. Mater. Chem. A
6
,
1340
1369
(
2018
).
8.
T.
Gao
,
T.
Ihara
,
S.
Grynning
,
B.P.
Jelle
, and
A.G.
Lien
,
Build. Environ.
95
405
413
(
2016
).
9.
C.
Buratti
,
F.
Merli
, and
E.
Moretti
,
Energy Build.
152
,
472
482
(
2017
).
10.
R.
Baetens
,
B. P.
Jelle
, and
A.
Gustavsen
,
Energy Build.
43
,
761
769
(
2011
).
11.
E.
Cuce
,
P. M.
Cuce
,
C. J.
Wood
, and
S. B.
Riffat
,
Renewable Sustainable Energy Rev.
34
,
273
299
(
2014
).
12.
A. A.
Pisal
and
A. V.
Rao
,
J. Porous. Mater.
23
,
1547
1556
(
2016
).
13.
G. A.
Sycheya
, “Nucleation and Crystal Growth in Phase Separated Glasses in the Lithium Silicate System” in
Crystallization and Materials Science of Modern Artificial and Natural Crystals
edited by
E.
Borisenko
(
InTech Open
,
2012
), pp.
23
48
.
14.
M. H.
Braga
,
N. S.
Grundish
,
A. J.
Murchisona
, and
J. B.
Goodenough
,
Energy Environ. Sci.
10
,
331
336
(
2017
).
15.
M. L.
Zheludkevich
,
I. M.
Salvado
, and
M. G. S.
Ferreira
,
J. Mater. Chem.
15
,
5099
5111
(
2005
).
16.
S.
Pandey
and
S. B.
Mishra
,
J. Sol-Gel Sci. Technol.
59
,
73
94
(
2011
).
17.
J. C.
Pouxviel
,
J. P.
Boilot
,
A.
Lecomte
, and
A.
Dauger
,
J. Physique
48
,
921
925
(
1987
).
18.
C. J.
Brinker
and
G. W.
Scherer
,
Sol-Gel Science The Physics and Chemistry of Sol-Gel Processing
(
Academic Press
,
New York
,
1990
), pp.
96
233
.
19.
E. J. A.
Pope
and
J. D.
Mackenzie
,
J. Non-Cryst. Solids
87
,
185
198
(
1986
).
20.
M. A.
Fardad
,
J. Mater. Sci.
35
,
1835
1841
(
2000
).
21.
D.
Collina
,
G.
Fornasari
,
A.
Rinaldo
,
F.
Trifirò
,
G.
Leofanti
,
G.
Paparatto
, and
G.
Petrini
,
Stud. Surf. Sci. Catal.
91
,
401
410
(
1995
).
22.
S. A.
Boussaa
,
A.
Kheloufi
,
N. B.
Zaourar
, and
S.
Bouachma
,
Acta Physica Polonica A.
132
,
1082
1086
(
2017
).
23.
S.
Silviana
,
B.
Jos
,
H.
Santosa
, and
S.
Sumardiono
,
J. Sci. Appl. Chem.
22
,
52
57
(
2019
).
24.
D. C.
Montgomery
,
Introduction to Statistical Quality Control
4th Edition (
John Wiley & Sons, Inc
.,
New York
,
2001
).
25.
T. M.
Temel
,
B. K.
İkizler
,
P.
Terzioğlü
,
S.
Yiicel
, and
Y. B.
Elalm1ş
,
J. Sol-Gel Sci Technol.
84
,
51
59
(
2017
).
26.
U. K. H.
Bangi
,
A. P.
Rao
,
H.
Hirashima
, and
A. V.
Rao
,
J. Sol-Gel Sci. Technol.
50
,
87
97
(
2009
).
27.
K.
Sinkò
,
J. Mater.
3
,
704
740
(
2010
).
28.
D.
Hayati
,
P.
Pardoyo
, and
C.
Azmityawati
,
J. Sci. Appl. Chem.
20
,
1
4
(
2017
).
This content is only available via PDF.