At present, the textile industry is increasing, so that consumer needs are increasing regarding textile dyes. And the use of natural dyes is currently very popular because it is environmentally friendly. One of the natural dyes that are often used in these products as a source of blue is Indigofera tinctoria L. because of its various potential. However, the extraction time required is very long in the conventional extraction process. Therefore, some researchers have proven that ultrasound-assisted extraction can accelerate and increase the extraction of results because ultrasonography can directly help the mechanism of matrix cell rupture through the mechanism of cavitation. Correlated with that, the extraction of Indigofera tinctoria L. dye using ultrasonic-assisted extraction was analysed by modelling with the response surface methodology with Box Behnken Design (BBD). The model obtained can represent the extraction process and show there are interactions between parameters on the results, but the F/S ratio has the most significant effect. In addition, the optimization model obtained the optimal condition extraction process with predicted values close to the actual results. Sample of extract were analysed using FT-IR

1.
T.
Pujilestari
, “Batik fabric dyeing process optimization using natural dyes tingi (Ceriops tagal) and Indigofera sp.,”
Dinamika Kerajinan dan Batik
, vol.
34
, no.
1
. pp.
53
62
,
2017
.
2.
S.
Wahyuningsih
,
L.
Wulandari
,
M. W.
Wartono
,
H.
Munawaroh
, and
A. H.
Ramelan
, “
The Effect of pH and Color Stability of Anthocyanin on Food Colorant
,”
IOP Conf. Ser. Mater. Sci. Eng.
, vol.
193
, no.
1
,
2017
, doi: .
3.
D.
Adalina
Y, “
Sumber Bahan Pewarna Alami sebagai Tinta Pidik Jari Pemilu
,”
Pus. Penelit. Dan Pengemb. Hutan Dan Konserv. Alam
,
2010
.
4.
G.
Rouhani
S
,
Alizadeh
N
,
Salimish
, “
Ultrasonic Assisted Extraction of natural pigments from rhizomes of Curcuma Longa L
.,”
J.Prog. Color. Color. Coatings.
, p.
2009
,
2009
.
5.
S.
Gala
,
M.
Mahfud
,
S.
Sumarno
, and
L.
Qadariyah
, “
Jurnal Bahan Alam Terbarukan The Extraction of Natural Dyes from Jackfruit Wood Waste ( Artocarpus heterophyllus Lamk) with Water Solvent by Using The Microwave Method
,”
2018
, doi: .
6.
H. S.
Kusuma
and
M.
Mahfud
, “
Kinetic studies on extraction of essential oil from sandalwood (Santalum album) by microwave air-hydrodistillation method
,”
Alexandria Eng. J.
, vol.
57
, no.
2
, pp.
1163
1172
,
2018
.
7.
M. A.
Bezerra
,
R. E.
Santelli
,
E. P.
Oliveira
,
L. S.
Villar
, and
L. A.
Escaleira
, “
Response Surface Methodology (RSM) as A Tool for Optimization in Analytical Chemistry
,”
Talanta
, vol.
76
, no.
5
, pp.
965
977
,
2008
, doi: .
8.
H. S.
Kusuma
,
A.
Altway
, and
M.
Mahfud
, “
An Optimization of Microwave Hydrodistillation Extraction Of Vetiver Oil Using A Face-Centered Central Composite Design
,”
J. Chem. Technol. Metall.
, vol.
54
, no.
4
, pp.
803
809
,
2019
.
9.
L. de C.
Gutierrez
,
Roldan
,
Ruiz Jimenez
J
, “
Ultrasound-assisted dynamic extraction of valuable compounds from aromatic plants and flowers as compared with steam distillation and superheated liquid extraction
,”
Dep. Anal. Chem.
, p.
14071
,
2008
.
10.
IlhemAit Amer
Meziane
,
N.
Bali
,
N. B.
Belblidia
,
N.
Abatzoglou
, “
The first-order model in the simulation of essential oil extraction kinetics
,”
J. Chem. Soc. Chem. Commun
, vol.
15
,
2019
.
11.
N. A. A.
Rahman
,
R.
Tajuddin
, and
S. M.
Tumin
, “
Optimization of Natural Dyeing Using Ultrasonic Method and Biomordant
,”
Int. J. Chem. Eng. Appl.
, vol.
4
, no.
3
, pp.
161
164
,
2013
, doi: .
12.
T. J.
Mason
and
J. P.
Lorimer
, “
Applied Sonochemistry: Uses of Power Ultrasound in
,”
Chemistry (Easton).
,
2004
.
13.
M.
Rouatbi
,
A.
Duquenoy
, and
P.
Giampaoli
, “
Extraction of the Essential Oil of Thyme and Black pepper by Superheated Steam
,”
J. Food Eng.
, vol.
78
, no.
2
, pp.
708
714
,
2007
, doi: .
14.
P. B.
Tayade
and
R. V.
Adivarekar
, “
Extraction of Indigo dye from Couroupita guianensisand its application on cotton fabric
,”
Fash. Text.
, vol.
1
, no.
1
, pp.
1
16
,
2014
, doi: .
This content is only available via PDF.
You do not currently have access to this content.