Bulk g-C3N4 catalysts are successfully prepared by a simple pyrolysis method at 550 °C. X-ray Powder Diffraction (XRD) and UV – Visible diffuse reflectance spectra techniques were used to analyze the samples. The performance of g- C3N4 on the photoreduction of Rodhamine B has carried out by various concentration of Rodhamine B. The result shows that the optimum condition were 100 mg g-C3N4 dilute on 60 ppm rodhamine B solution, for 90 minutes irradiation using Black Light Blue lamp. This condition is able to degrade 87,45% of rhodamine B pollutant.
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