Detection of urea is generally accomplished by urea biosensors, which necessitates the immobilization of enzymes (i.e. urease), hence limiting their utility. In this report, we have demonstrated the non-enzymatic electrochemical detection of urea by means of CdV2O4-V6O13 micro-flowers (CdV2O4-V6O13 MFs). The physicochemical properties of this material were revealed by different characterization methods, which include the powder X-ray diffraction (PXRD) technique, field-emission scanning electron microscopy (FE-SEM), energy dispersive X-ray spectroscopy (EDX) and Fourier transform infrared (FT-IR) spectroscopy. Finally this material was successfully employed for the non-enzymatic detection of urea by electrochemical method. This detection ability can be accredited to the high sensitivity, large electroactive surface area and unique morphology of CdV2O4-V6O13 MFs.

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