The pursuit for cheap, eco-friendly and greener starting material that is suitable for the synthesis of zeolite directed the attention of researchers on adaptation of kaolinite minerals for zeolite production. In view of that, a low grade kaolin which is obtained from Mersing area of Johor state in peninsular Malaysia was utilized for the synthesis of zeolite though hydrothermal process at lower temperature without any addition of Structural Directing Agent (SDA). The synthesized zeolite was then analyzed using X-ray diffraction and scanning electron microscopy to evaluate the potentials of the process and the product. The outcome of the analysis suggests that the Mersing kaolin is suitable for zeolite production and the metakaolinization at 700 °C for 2 hours improves the raw material reactivity and invariably influences the synthesis process and the product. The synthesis process conducted as a low temperature (90 °C) for 9 hours was able to produce zeolites of good crystallinity. However, the presence of secondary phases informed the effect of the accompanied impurities.

1.
T.
Abdullahi
,
Z.
Harun
, and
M.H.D.
Othman
,
Adv. Powder Technol.
28
,
1827
1840
(
2017
).
2.
E.
Johnson
and
S.E.
Arshad
,
Appl. Clay Sci.
97
,
215
221
(
2014
).
3.
N.M.
Musyoka
,
R.
Missengue
,
M.
Kusisakana
and
L.F.
Petrik
,
Appl. Clay Sci.
97
,
182
186
(
2014
).
4.
S.
Chandrasekhar
and
P.
Pramada
,
J. Porous Mater.
6
,
283
297
(
1999
).
5.
S.M.
Holmes
,
S.H.
Khoo
and
A.S.
Kovo
,
Green Chem.
13
,
1152
1154
, (
2011
).
6.
R.W.
Broach
and
R.M.
Kirchner
,
Microporous Mesoporous Mater.
143
,
398
400
(
2011
).
7.
M.
Gougazeh
and
J.C.
Buhl
,
J. Assoc. Arab Univ. Basic Appl. Sci.
15
,
35
42
(
2014
).
8.
T.
Abdullahi
,
Jurnal Teknologi
77
,
9
16
(
2015
).
9.
R.
Babalola
,
Development and Characterization of Zeolitey From A Nigerian Local Raw Material
,
Covenant University
,
Nigeria
,
2015
.
10.
H.
Baioumy
and
A.R.
Ibrahim
, in
Annu. Int. Conf. Geol. Earth Sci.
(
2012
), pp.
133
140
.
11.
K.S.
Ariffin
,
H.A.
Rahman
,
H.
Hussin
, and
K.A.A.
Hadi
,
Bull. Geol. Soc. Malaysia
54
,
9
16
(
2008
).
12.
M.G.D.
Malaysia
,
Malaysian Minerals Yearbook 2012
(
2012
).
13.
S.
Chandrasekhar
and
P.
Pramada
,
Microporous Mesoporous Mater.
108
,
152
161
(
2008
).
14.
L.
Ayele
,
E.
Pérez
,
Á.
Mayoral
,
Y.
Chebude
and
I.
Díaz
,
J. Chem. Technol. Biotechnol.
93
,
146
154
(
2018
).
15.
H.
Feng
,
C.
Li
and
H.
Shan
,
Catal. Letters.
129
,
71
78
(
2009
).
16.
S.
Chandrasekhar
,
Clay Miner.
31
,
253
261
(
1996
).
17.
J.
Kugbe
,
N.
Matsue
and
T.
Henmi
,
J. Hazard. Mater.
164
,
929
935
(
2009
).
18.
M.M.J.
Treacy
and
J.B.
Higgins
,
Collection of Simulated XRD Powder Patterns for Zeolites Fifth (5th) Revised Edition
(
Elsevier
,
2007
).
This content is only available via PDF.
You do not currently have access to this content.