Gallosilicate cancrinite with carbonate anion, Na8[GaSiO4]6(CO3)1.72(H2O)5 has been synthesized at low temperature by hydrothermal method (373 K). The white crystalline cancrinite powder was characterized by IR, X-ray powder diffraction, TGA, SEM, and MAS NMR. Crystal structure was refined in the space group P63, from X-ray powder diffraction data using Rietveld refinement method with a = 12.5899 Å, c = 5.1424 Å. The average Al-O bond distance is 1.8109 Å and Si-O bond distance is 1.5847 Å, while the T-O-T angle is found to be 138.793°. TGA shows thermal behavior of the carbonate anion inside the cancrinite cages. The single resonance line in the 29Si spectrum confirms strictly alternating order of Ga and Si in the framework. The SEM picture shows hexagonal needle shaped structures.
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15 January 2019
STATE-OF-THE-ART TRENDS OF SCIENTIFIC RESEARCH OF ARTIFICIAL AND NATURAL NANOOBJECTS, STRANN-2018
17–19 October 2018
Moscow, Russia
Research Article|
January 15 2019
Synthesis and characterization of gallo-silicate carbonate cancrinite Available to Purchase
S. G. Wakchaure
Department of Chemistry, Pune Vidyarthi Griha’s College of Engineering
, Nashik 422005, India
Corresponding author: email:- [email protected]
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S. G. Wakchaure
Department of Chemistry, Pune Vidyarthi Griha’s College of Engineering
, Nashik 422005, India
Corresponding author: email:- [email protected]
AIP Conf. Proc. 2064, 030017 (2019)
Citation
S. G. Wakchaure; Synthesis and characterization of gallo-silicate carbonate cancrinite. AIP Conf. Proc. 15 January 2019; 2064 (1): 030017. https://doi.org/10.1063/1.5087679
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