Synthesis of 5-methyl-1,2,4-triazolo[1,5-a]pyrimidin-7(4H)-one - a semi-product of the synthesis of antiviral drug triazide® in the conditions of microwave excitation

Baklykov, Artem V.; Rusinov, Gennady L.; Artem’ev, Grigory A.; Kopchuk, Dmitry S.; Zyryanov, Grigory V.; Rusinov, Vladimir L.; Charushin, Valery N.

doi:10.1063/1.5087337

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Research Article| January 11 2019

Synthesis of 5-methyl-1,2,4-triazolo[1,5-a]pyrimidin-7(4H)-one - a semi-product of the synthesis of antiviral drug triazide® in the conditions of microwave excitation

Artem V. Baklykov;

Artem V. Baklykov ^a)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

^a)Corresponding author: art.baklykov@gmail.com

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Gennady L. Rusinov;

Gennady L. Rusinov ^b)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

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Grigory A. Artem’ev;

Grigory A. Artem’ev ^c)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

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Dmitry S. Kopchuk;

Dmitry S. Kopchuk ^d)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

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Grigory V. Zyryanov;

Grigory V. Zyryanov ^e)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

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Vladimir L. Rusinov;

Vladimir L. Rusinov ^f)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

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Valery N. Charushin

Valery N. Charushin ^g)

1

I. Ya. Postovsky Institute of Organic Synthesis of RAS (Ural Division)

, 22/20, S. Kovalevskoy/Akademicheskaya St., Yekaterinburg, 62099,

Russian Federation

2

Ural Federal University

, 19, Mira St., Yekaterinburg, 62000,

Russian Federation

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Author & Article Information

^a)Corresponding author: art.baklykov@gmail.com

^b)

^c)

^d)

^e)

^f)

^g)

charushin@ios.uran.ru

AIP Conf. Proc. 2063, 040005 (2019)

https://doi.org/10.1063/1.5087337

5-Methyl-1,2,4-triazolo[1,5-a]pyrimidine-7(4H)-one was synthesized (the intermediate product for the syn-thesis of the antiviral drug Triazide®) under microwave radiation. Conversion of the starting reagents to the target product reached 95% due to experimentally selected conditions.

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Synthesis of 5-methyl-1,2,4-triazolo[1,5-a]pyrimidin-7(4H)-one - a semi-product of the synthesis of antiviral drug triazide® in the conditions of microwave excitation

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