Intumescent coating is a method of passive fireproofing that is applied to structural members of building and helps prevent the fire heat from reaching the structure. The issue with fibre reinforced intumescent coating was that the fibre tend to coagulate when the coating was applied to the structure because they did not have a good dispersion. In the current study, a coating was prepared with basic components of ammonium polyphosphate (APP), expandable graphite, and melamine (MEL) in an epoxy resin base with boric acid as additive. Basalt fibres were used as reinforcements with BYK-9920 as the dispersing agent and their effects on thermal properties were investigated. The coating was applied by brushing onto steel substrates of 100 cm2 and 25 cm2 area. The effects of different weight percentage of the reinforcements were studied by performing fire test and furnace test for heat shielding effect and char expansion. Further analysis was performed by thermogravimetric analysis (TGA) for residual weight and thermal stability. From the TGA, the formulations showed increase in final residual weight. The coatings were able to expand up to 635% and reduce the substrate temperature from 1000°C to 180°C.

1.
M.
Jimenez
,
S.
Duquesne
, and
S.
Bourbigot
, “
Intumescent fire protective coating: Toward a better understanding of their mechanism of action
,”
Thermochimica Acta
, vol.
449
, pp.
16
26
,
2006
.
2.
A.
Beheshti
and
S. Z.
Heris
, “
Is MWCNT a good synergistic candidate in APP–PER–MEL intumescent coating for steel structure?
,”
Progress in Organic Coatings
, vol.
90
, pp.
252
257
,
2016
.
3.
M.
Jimenez
,
S.
Duquesne
, and
S.
Bourbigot
, “
Multiscale experimental approach for developing high-performance intumescent coatings
,”
Industrial & engineering chemistry research
, vol.
45
, pp.
4500
4508
,
2006
.
4.
R. G.
Puri
and
A. S.
Khanna
, “
Effect of cenospheres on the char formation and fire protective performance of water-based intumescent coatings on structural steel
,”
Progress in Organic Coatings
, vol.
92
, pp.
8
15
, 2016/03/01/
2016
.
5.
P.
Banibayat
and
A.
Patnaik
, “
Variability of mechanical properties of basalt fiber reinforced polymer bars manufactured by wet-layup method
,”
Materials & Design (1980-2015)
, vol.
56
, pp.
898
906
,
2014
.
6.
V.
Fiore
,
T.
Scalici
,
G.
Di Bella
, and
A.
Valenza
, “
A review on basalt fibre and its composites
,”
Composites Part B: Engineering
, vol.
74
, pp.
74
94
,
2015
.
7.
M.
Gomez-Mares
,
A.
Tugnoli
,
G.
Landucci
,
F.
Barontini
, and
V.
Cozzani
, “
Behavior of intumescent epoxy resins in fireproofing applications
,”
Journal of analytical and applied pyrolysis
, vol.
97
, pp.
99
108
,
2012
.
8.
K. P.
Nørgaard
,
K.
Dam-Johansen
,
P.
Català
, and
S.
Kiil
, “
Investigation of char strength and expansion properties of an intumescent coating exposed to rapid heating rates
,”
Progress in Organic Coatings
, vol.
76
, pp.
1851
1857
, 2013/12/01/
2013
.
9.
M. C.
Yew
and
N. H. Ramli
Sulong
, “
Fire-resistive performance of intumescent flame-retardant coatings for steel
,”
Materials & Design
, vol.
34
, pp.
719
724
, 2012/02/01/
2012
.
10.
Q. F.
Gillani
,
F.
Ahmad
,
M. I. A.
Mutalib
,
P. S.
Melor
,
S.
Ullah
, and
A.
Arogundade
, “
Effect of Dolomite Clay on Thermal Performance and Char Morphology of Expandable Graphite Based Intumescent Fire Retardant Coatings
,”
Procedia Engineering
, vol.
148
, pp.
146
150
, //
2016
.
11.
W. F.
Mohamad
,
F.
Ahmad
, and
S.
Ullah
, “
Effect of inorganic fillers on thermal performance and char morphology of intumescent fire retardant coating
,”
Asian Journal of Scientific Research
, vol.
6
, p.
263
,
2013
.
12.
S.
Ullah
,
F.
Ahmad
,
A. M.
Shariff
, and
M. A.
Bustam
, “
Synergistic effects of kaolin clay on intumescent fire retardant coating composition for fire protection of structural steel substrate
,”
Polymer Degradation and Stability
, vol.
110
, pp.
91
103
, 2014/12/01/
2014
.
13.
G.
Li
,
G.
Liang
,
T.
He
,
Q.
Yang
, and
X.
Song
, “
Effects of EG and MoSi 2 on thermal degradation of intumescent coating
,”
Polymer degradation and stability
, vol.
92
, pp.
569
579
,
2007
.
14.
G.
Li
,
J.
Yang
,
T.
He
,
Y.
Wu
, and
G.
Liang
, “
An investigation of the thermal degradation of the intumescent coating containing MoO 3 and Fe 2 O 3
,”
Surface and coatings Technology
, vol.
202
, pp.
3121
3128
,
2008
.
15.
J. H.
Koo
, “
Thermal Characteristics Comparison of Two Fire Resistant Materials
,”
Journal of Fire Sciences
, vol.
15
, pp.
203
221
,
1997
.
16.
N.
Amir
,
A. A.
Majid
, and
F.
Ahmad
, “
Effects of Hybrid Fibre Reinforcement on Fire Resistance Performance and Char Morphology of Intumescent Coating
,” in
MATEC Web of Conferences
,
2016
.
17.
N.
Amir
,
F.
Ahmad
, and
P.
Megat-Yusoff
, “
Study on the fibre reinforced epoxy-based intumescent coating formulations and their char characteristics
,”
Journal of Applied Sciences
, vol.
11
, pp.
1678
1687
,
2011
.
18.
N.
Amir
,
F.
Ahmad
, and
P. S. M.
Megat-Yusoff
, “
Mechanisms of char strengthening in the fibre reinforced intumescent coatings
,”
Journal of Applied Sciences
, vol.
12
, p.
2459
,
2012
.
19.
S. E.
Artemenko
, “
Polymer Composite Materials Made from Carbon, Basalt, and Glass Fibres. Structure and Properties
,”
Fibre Chemistry
, vol.
35
, pp.
226
229
, May 01
2003
.
20.
R.
Subramanian
and
H.
Austin
, “
Silane coupling agents in basalt-reinforced polyester composites
,”
International Journal of Adhesion and Adhesives
, vol.
1
, pp.
50
54
,
1980
.
21.
T.
Deák
and
T.
Czigány
, “
Chemical composition and mechanical properties of basalt and glass fibers: a comparison
,”
Textile Research Journal
, vol.
79
, pp.
645
651
,
2009
.
22.
S.
Feih
and
A. P.
Mouritz
, “
Tensile properties of carbon fibres and carbon fibre–polymer composites in fire
,”
Composites Part A: Applied Science and Manufacturing
, vol.
43
, pp.
765
772
, 2012/05/01/
2012
.
23.
S.
Feih
,
A.
Mouritz
,
Z.
Mathys
, and
A.
Gibson
, “
Tensile Strength Modeling of Glass Fiber—Polymer Composites in Fire
,”
Journal of composite materials
, vol.
41
, pp.
2387
2410
,
2007
.
24.
A. N.
Mengal
,
S.
Karuppanan
, and
A. A.
Wahab
, “
Basalt carbon hybrid composite for wind turbine rotor blades: A Short Review
,” in
Advanced Materials Research
,
2014
, pp.
67
73
.
25.
Y.
Muhammad
,
A.
Norlaili
,
A.
Faiz
, and
N. S.
Rodzhan
, “
Effect of basalt fibres reinforcement and aluminum trihydrate on the thermal properties of intumescent fire retardant coatings
,”
IOP Conference Series: Materials Science and Engineering
, vol.
226
, p.
012185
,
2017
.
26.
H.
Aziz
and
F.
Ahmad
, “
Effects from nano-titanium oxide on the thermal resistance of an intumescent fire retardant coating for structural applications
,”
Progress in Organic Coatings
, vol.
101
, pp.
431
439
, 12//
2016
.
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