Virgin Coconut Oil (VCO) has been applied in many application and products. Formation of microemulsion region with surfactant was investigated by using phase diagram. The surfactants used are igepal CO-520 and tween 80. The studies showed that formation of microemulsion region were dependent on the behaviour of the surfactant toward VCO. The result showed that microemulsion regions were present in igepal CO-520 system formed a larger water-in-oil microemulsion region compared to tween 80 system. Certain weight ratios of VCO to surfactants were studied by using evaporation test in order to study the water loss of the microemulsion in ambient condition. The evaporation rate of samples was varies depending their compositon of VCO, surfactant and water.

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