Hydroxyapatite (Ca10 (PO4)6 (OH)2, HAP) is the main inorganic component of the hard tissues in bones and also important material for orthopedic and dental implant applications. Nano HAP is of great interest due to its various bio-medical applications. In the present work the nano HAP was synthesized by using surfactant mediated approach. Structure and morphology of the synthesized nano HAP was examined by the Powder XRD and TEM. Impedance study was carried out on pelletized sample in a frequency range of 100Hz to 20MHz at room temperature. The variation of dielectric constant, dielectric loss, and a.c. conductivity with frequency of applied field was studied. The Nyquist plot as well as modulus plot was drawn. The Nyquist plot showed two semicircle arcs, which indicated the presence of grain and grain boundary effect in the sample. The typical behavior of the Nyquist plot was represented by equivalent circuit having two parallel RC combinations in series.

1.
V. C.
Gshalaev
and
A.C.
Demirchan
,
Hydroxyapatite: Synthesis, Properties and Applications
(
Nova Science Publisher
,
New York
,
2012
).
2.
P.
Frayssinet
,
P.
Bonnevialle
,
J.
Autefage
,
P.
Sharrock
,
G.
Bonel
,
Bioartificial Hydroxylapatite Implants Limb Salvage
(
Springer
,
Berlin Heidelberg
,
1991
).
3.
K. P.
Tank
,
Nano Hydroxyapatite and Silver Doped nano Hydroxyapatite
(
Scholar’s Press
,
Saarbrücken, Germany
,
2014
)
4.
A. A.
Marino
,
R. O.
Becker
, and
C. H.
Bachman
,
Phys. Med. Biol.
12
,
367
378
(
1967
).
5.
R. T.
Kuzyk
and
E. H.
Schemitsch
,
Indian J. Orthop.
43
(
2
),
127
131
(
2009
).
6.
J. C.
Elliot
,
Structure and Chemistry of the Apatites and Other Calcium Orthophosphates
(
Elsevier
,
Amsterdam
,
1994
)
7.
K. P.
Tank
,
P.
Sharma
,
D. K.
Kanchan
and
M. J.
Joshi
,
Cryst. Res. Technol.
46
(
12
),
1309
1316
(
2011
).
8.
J. P.
Gittings
,
C. R.
Bowen
,
A. C. E.
Dent
,
I. G.
Turner
,
F. R.
Baxter
and
J. B.
Chaudhuri
,
Acta. Biomaterialia
5
,
743
754
(
2009
).
9.
D. K.
Pradhan
,
R. N. P.
Chaudhary
and
B. K.
Samantary
,
Inter. J. of Electrochem. Sci.
3
,
597
608
(
2008
).
10.
P. U.
Sharma
, “
Investigations on the effect of thermal history, particle size and SHI irradiation on some physical properties of Y3+-substituted YIG
”,
Saurashtra University
, Ph.D. Thesis,
2009
.
11.
S. R.
Vasant
, “
Synthesis and Characterization of Pure and Doped Calcium Pyrophosphate Nano-Particles
”,
Saurashtra University
, Ph.D. Thesis,
2015
.
12.
O.
Kaygilia
,
S. V.
Dorozhkin
,
T.
Atesa
,
A. A.
Al-Ghamdic
,
F.
Yakuphanoglua
,
Ceram. Int.
.
40
9395
9402
(
2014
).
13.
P. R.
Das
,
S.
Behera
,
R.
Padhee
,
P.
Nayak
,
R. N. P.
Chaudhary
,
J. of Adv. Ceram.
1
(
3
),
232
240
(
2012
).
14.
A.
Molak
,
E.
Talik
,
M.
Kruczek
,
Mater Sci Eng B
,
128
,
16
24
(
2006
).
15.
M. Harish
Bhat
,
M.
Ganguli
and
K. J.
Rao
,
Bull. Mater. Sci.
26
(
4
),
413
407
(2003).
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