The WC-C peritectic fixed point, nominal melting and freezing temperature 2747 °C, shows extremely good metrological potential. Elsewhere, we published a prototype scale comparison of the ITS-90 between NPL, NIM and CEM, using high temperature eutectic fixed points (HTFPs) of Co-C (1324 °C), Pt-C (1738 °C), and Re-C (2474 °C). In this paper we present the further results of the bilateral comparison of the ITS-90 at an even higher temperature, 2747 °C, between NIM and NPL using WC-C peritectic fixed points. A NIM single zone high temperature furnace, model Chino IR-80, was modified to extend its temperature to 2800 °C. Then, an NPL researcher, on secondment to NIM, filled two WC-C cells in the modified furnace in a vertical position. The two WC-C cells were then realized in the same furnace, in an horizontal position. Their melting temperatures, defined by the inflection point of the melting curves, were measured by a linear pyrometer, model NIM-PSP. NIM's ITS-90 scale was assigned to the two cells, which were then transported to NPL. The realization of NPL's ITS-90 was then assigned to the two cells by using a model HT9500 Thermogauge furnace to realize the fixed points and a linear pyrometer, model LP3, to determine their temperature. The difference from the mean value of the NIM and NPL ITS-90 values for the WC-C points was derived. This allowed us to compare ITS-90 as realized by the two institutes and to determine the uncertainty in the scale comparison.
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11 September 2013
TEMPERATURE: ITS MEASUREMENT AND CONTROL IN SCIENCE AND INDUSTRY, VOLUME 8: Proceedings of the Ninth International Temperature Symposium
19–23 March 2012
Los Angeles, California, USA
Research Article|
September 11 2013
Bilateral ITS-90 comparison at WC-C peritectic fixed point between NIM and NPL
W. Dong;
W. Dong
NIM, Bei San Huan Dong Lu No. 18, Beijing, 100013,
China
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D. H. Lowe;
D. H. Lowe
National Physical Laboratory, Hampton Road, Teddington, TW11 0LW,
United Kingdom
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X. Lu;
X. Lu
NIM, Bei San Huan Dong Lu No. 18, Beijing, 100013,
China
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G. Machin;
G. Machin
National Physical Laboratory, Hampton Road, Teddington, TW11 0LW,
United Kingdom
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Z. Yuan;
Z. Yuan
NIM, Bei San Huan Dong Lu No. 18, Beijing, 100013,
China
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T. Wang;
T. Wang
NIM, Bei San Huan Dong Lu No. 18, Beijing, 100013,
China
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P. Bloembergen;
P. Bloembergen
NIM, Bei San Huan Dong Lu No. 18, Beijing, 100013,
China
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C. Xiao
C. Xiao
Beijing University of Technology, Beijing, 100022,
China
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AIP Conf. Proc. 1552, 786–790 (2013)
Citation
W. Dong, D. H. Lowe, X. Lu, G. Machin, Z. Yuan, T. Wang, P. Bloembergen, C. Xiao; Bilateral ITS-90 comparison at WC-C peritectic fixed point between NIM and NPL. AIP Conf. Proc. 11 September 2013; 1552 (1): 786–790. https://doi.org/10.1063/1.4821408
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